Preparation of substituted cyclopentadienyl ligands by nucleophilic addition to substituted fulvenes
By modifing the procedure reported by Stone and Little, we have been able to make substituted fulvenes on a large scale and maintain good yield. Treatment of 6-tert-butylfulvene with lithium diethylamine gave, upon work-up, neopentylcyclopentadiene in 83% yield. Treatment of neopentylcyclopentadiene...
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DigitalCommons@Robert W. Woodruff Library, Atlanta University Center
1990
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| Online Access: | http://digitalcommons.auctr.edu/dissertations/3188 http://digitalcommons.auctr.edu/cgi/viewcontent.cgi?article=4005&context=dissertations |