Structural and mechanistic study of monoalkyl diazenes. Synthesis, characterization, and reactivity of 1,6-didehydro[10]annulene
<p>Methodology for the preparation of allenes from propargylic hydrazine precursors under mild conditions is described. Oxidation of the propargylic hydrazines, which can be readily prepared from propargylic alcohols, with either of two azo oxidants, diethyl azodicarboxylate (DEAD) or 4-met...
Internet
https://thesis.library.caltech.edu/7647/1/Finney%20%201994.pdfFinney, Nathaniel S. (1994) Structural and mechanistic study of monoalkyl diazenes. Synthesis, characterization, and reactivity of 1,6-didehydro[10]annulene. Dissertation (Ph.D.), California Institute of Technology. doi:10.7907/pjpf-6x38. https://resolver.caltech.edu/CaltechTHESIS:04302013-092335648 <https://resolver.caltech.edu/CaltechTHESIS:04302013-092335648>