Thiosilanes as thioketalization reagents
Thiosilanes react efficiently with simple aldehydes and ketones when catalyzed with ZnI_2 to produce thioacetals and thioketals. Steroidal diketones were thioketalized with yields and selectivity superior to other methods when allowed to react with thiosilanes and ZnI_2. The overall thioketalizat...
Internet
https://thesis.library.caltech.edu/5692/1/Nesbitt_sl_1977.pdfNesbitt, Stephen L. (1977) Thiosilanes as thioketalization reagents. Master's thesis, California Institute of Technology. doi:10.7907/CDYJ-S314. https://resolver.caltech.edu/CaltechTHESIS:04062010-085409602 <https://resolver.caltech.edu/CaltechTHESIS:04062010-085409602>