I. Synthesis of methylenecyclobutane from pentaerythrityl chloride. II. The attempted synthesis of cyclobutane. III. Reinvestigation of the synthesis of spiroheptanedicarboxylic acid
I. THE SYNTHESIS OF METHYLENECYCLOBUTANE FROM PENTAERYTHRITYL CHLORIDE A new method for preparing methylenecyclobutane is described in which the starting material is pentaerythrityl tetrachloride. Pentaerythrityl chloride is dechlorinated by zinc dust in the presence of sodium iodide and sodium car...
Internet
https://thesis.library.caltech.edu/3941/1/Winniford_rs_1948.pdfWinniford, Robert Stanley (1948) I. Synthesis of methylenecyclobutane from pentaerythrityl chloride. II. The attempted synthesis of cyclobutane. III. Reinvestigation of the synthesis of spiroheptanedicarboxylic acid. Master's thesis, California Institute of Technology. doi:10.7907/ZMYX-Z369. https://resolver.caltech.edu/CaltechETD:etd-10062005-083407 <https://resolver.caltech.edu/CaltechETD:etd-10062005-083407>