The preparation and study of new metal binding reagents
New phosphine ligands which also contained crown ether groups were synthesized by condensing two main reagents. Reagent A was Ph2P(CH2)3NH2 and it was prepared by reductingPh2P(CH2)2CN with LiALH4 in diethyl ether. Ph2P(CH2)2CN is obtained by reacting Ph2PH and CH2=C(H)CN in a Michael-type reaction....
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| Format: | Others |
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2011
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| Online Access: | http://cardinalscholar.bsu.edu/handle/handle/184042 http://liblink.bsu.edu/uhtbin/catkey/722440 |