An Attempt to Prepare Trinuclear Tungsten Oxoalkoxides [BzMe3N]3[W3O8(OMe)5]
From the reaction between WO2(OMe)2, [BzMe3N]2WO4 and [BzMe3N](OMe) in the ratio of 2:1:1 in MeOH produced [BzMe3N]2[Na2W4O12(OMe)4(MeOH)6].6MeOH. Suitable crystals for X-ray chrystallographic studies were obtained from hot mixture of methanol-acetonitrile solution. The I.R., 1H-NMR, and microanalys...
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| Format: | Article |
| Language: | English |
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Universitas Indonesia
2003-04-01
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| Series: | Makara Seri Sains |
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| Online Access: | http://journal.ui.ac.id/science/article/view/290/286 |