Synthesis and crystal structures of three new benzotriazolylpropanamides

Synthesis and crystal structures of three new benzotriazolylpropanamides

The base-catalyzed Michael addition of 2-methylacrylamide to benzotriazole afforded 3-(1H-benzotriazol-1-yl)-2-methylpropanamide, C10H12N4O (1), in 32% yield in addition to small amounts of isomeric 3-(2H-benzotriazol-2-yl)-2-methylpropanamide, C10H12N4O (2). In a similar manner, 3-(1H-benzotriazol-...

Full description

Bibliographic Details
Main Authors: Donna S. Amenta, Phil Liebing, Julia E. Biero, Robert J. Sherman, John W. Gilje, Frank T. Edelmann
Format: Article
Language:English
Published: International Union of Crystallography 2017-06-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
crystal structure
acrylamide
benzotriazole
benzotriazolylpropanamide
hydrogen bond
π–π stacking
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989017007472

Internet

http://scripts.iucr.org/cgi-bin/paper?S2056989017007472

Similar Items