Synthesis and structure of 2,4,6-tricyclobutyl-1,3,5-trioxane

The synthesis and structure of 2,4,6,-tricyclobutyl-1,3,5-trioxane, C15H24O3 1, is described. It was formed in 39% yield during the work-up of the Swern oxidation of cyclobutylmethanol and may serve as a stable precursor of the cyclobutane carbaldehyde. The molecule of 1 occupies a special position...

Full description

Bibliographic Details
Main Authors: Sergey V. Shorunov, Maxim V. Bermeshev, Dmitry V. Demchuk, Yulia V. Nelyubina
Format: Article
Language:English
Published: International Union of Crystallography 2019-11-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
Online Access:http://scripts.iucr.org/cgi-bin/paper?S205698901900896X