Rerefinement of poly[diaquabis(μ3-2-methylpropanoato-κ4O:O,O′:O′)bis(μ3-2-methylpropanoato-κ3O:O:O)(μ2-2-methylpropanoato-κ3O:O,O′)(2-methylpropanoato-κ2O,O′)trilead(II)]
The crystal structure of the title complex, [Pb3(C4H7O2)6(H2O)2]n, was redetermined on basis of modern CCD-based single-crystal X-ray data at 120 K. The current study basically confirms the previous report [Fallon et al. (1997). Polyhedron, 16, 19–23] at 190 K, but with higher accuracy and precision...
| Main Authors: | , |
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| Format: | Article |
| Language: | English |
| Published: |
International Union of Crystallography
2020-10-01
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| Series: | IUCrData |
| Subjects: | |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S2414314620013115 |