Synthesis of Isotope Labeled Protocatechuic Acid-(13COOH)

Synthesis of Isotope Labeled Protocatechuic Acid-(13COOH)

A novel synthesis method of protocatechuic acid-(13COOH) was designed. 3,4-dimethoxy bromobenzene as raw material, Grignard reagent was prepared by Grignard reaction, then passed through the 13C labeled 13CO2 gas, the intermediate 3,4-dimethoxy benzoic acid-(13COOH) was prepared. The crude product w...

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Bibliographic Details
Main Author:	XU Jianfei;LIU Zhanfeng;LU Weijing;LEI Wen;HOU Jie;DU Xiaoning
Format:	Article
Language:	zho
Published:	Editorial Board of Journal of Isotopes 2020-12-01
Series:	Journal of Isotopes
Subjects:	13c-labeled protocatechuic acid grignard reaction
Online Access:	http://www.tws.org.cn/CN/abstract/abstract1823.shtml

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