Synthesis of Isotope Labeled Protocatechuic Acid-(13COOH)
A novel synthesis method of protocatechuic acid-(13COOH) was designed. 3,4-dimethoxy bromobenzene as raw material, Grignard reagent was prepared by Grignard reaction, then passed through the 13C labeled 13CO2 gas, the intermediate 3,4-dimethoxy benzoic acid-(13COOH) was prepared. The crude product w...
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Format: | Article |
Language: | zho |
Published: |
Editorial Board of Journal of Isotopes
2020-12-01
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Series: | Journal of Isotopes |
Subjects: | |
Online Access: | http://www.tws.org.cn/CN/abstract/abstract1823.shtml |