Influence of Freezing and Different Drying Methods on Volatile Profiles of Strawberry and Analysis of Volatile Compounds of Strawberry Commercial Jams

Strawberry is the most consumed berry fruit worldwide due to its unique aroma and flavor. Drying fruits to produce a powder represents one of the possible conservation methods to extend their shelf-life. The aim of the present study was to compare the influence of freezing and different drying metho...

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Main Authors: Doaa Abouelenein, Ahmed M. Mustafa, Simone Angeloni, Germana Borsetta, Sauro Vittori, Filippo Maggi, Gianni Sagratini, Giovanni Caprioli
Format: Article
Language:English
Published: MDPI AG 2021-07-01
Series:Molecules
Subjects:
Online Access:https://www.mdpi.com/1420-3049/26/14/4153
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spelling doaj-3d35883959bb440381424e8cbd388a5b2021-07-23T13:56:15ZengMDPI AGMolecules1420-30492021-07-01264153415310.3390/molecules26144153Influence of Freezing and Different Drying Methods on Volatile Profiles of Strawberry and Analysis of Volatile Compounds of Strawberry Commercial JamsDoaa Abouelenein0Ahmed M. Mustafa1Simone Angeloni2Germana Borsetta3Sauro Vittori4Filippo Maggi5Gianni Sagratini6Giovanni Caprioli7School of Pharmacy, University of Camerino, Via Sant’Agostino 1, 62032 Camerino, ItalySchool of Pharmacy, University of Camerino, Via Sant’Agostino 1, 62032 Camerino, ItalySchool of Pharmacy, University of Camerino, Via Sant’Agostino 1, 62032 Camerino, ItalySchool of Pharmacy, University of Camerino, Via Sant’Agostino 1, 62032 Camerino, ItalySchool of Pharmacy, University of Camerino, Via Sant’Agostino 1, 62032 Camerino, ItalySchool of Pharmacy, University of Camerino, Via Sant’Agostino 1, 62032 Camerino, ItalySchool of Pharmacy, University of Camerino, Via Sant’Agostino 1, 62032 Camerino, ItalySchool of Pharmacy, University of Camerino, Via Sant’Agostino 1, 62032 Camerino, ItalyStrawberry is the most consumed berry fruit worldwide due to its unique aroma and flavor. Drying fruits to produce a powder represents one of the possible conservation methods to extend their shelf-life. The aim of the present study was to compare the influence of freezing and different drying methods on the volatile profile of strawberry using the HS-SPME/GC–MS method, in addition to analysis of strawberry jam volatiles. A total of 165 compounds were identified, accounting for 85.03–96.88% of the total volatile compositions. Results and PCA showed that freezing and each drying process affected the volatile profile in a different way, and the most remarkable representative differential volatiles were ethyl hexanoate, hexyl acetate, (<i>E</i>)-2-hexenyl acetate, mesifurane, (<i>E</i>)-nerolidol, <i>γ</i>-decalactone, 1-hexanol, and acetoin. Shade air-dried, frozen, freeze-dried, and oven-dried 45 °C samples retained more of the fruity and sweet aromas of strawberry, representing more than 68% of the total aroma intensity according to the literature. In contrast, the microwave-drying method showed drastic loss of fruity esters. Strawberry jams demonstrated complete destruction of esters and alcohols in most jams, while terpenes were significantly increased. These findings help better understand the aroma of strawberry and provide a guide for the effects of drying, freezing, and jam processing.https://www.mdpi.com/1420-3049/26/14/4153strawberryaromavolatile organic compoundsdrying methodsfreezingcommercial jams
collection DOAJ
language English
format Article
sources DOAJ
author Doaa Abouelenein
Ahmed M. Mustafa
Simone Angeloni
Germana Borsetta
Sauro Vittori
Filippo Maggi
Gianni Sagratini
Giovanni Caprioli
spellingShingle Doaa Abouelenein
Ahmed M. Mustafa
Simone Angeloni
Germana Borsetta
Sauro Vittori
Filippo Maggi
Gianni Sagratini
Giovanni Caprioli
Influence of Freezing and Different Drying Methods on Volatile Profiles of Strawberry and Analysis of Volatile Compounds of Strawberry Commercial Jams
Molecules
strawberry
aroma
volatile organic compounds
drying methods
freezing
commercial jams
author_facet Doaa Abouelenein
Ahmed M. Mustafa
Simone Angeloni
Germana Borsetta
Sauro Vittori
Filippo Maggi
Gianni Sagratini
Giovanni Caprioli
author_sort Doaa Abouelenein
title Influence of Freezing and Different Drying Methods on Volatile Profiles of Strawberry and Analysis of Volatile Compounds of Strawberry Commercial Jams
title_short Influence of Freezing and Different Drying Methods on Volatile Profiles of Strawberry and Analysis of Volatile Compounds of Strawberry Commercial Jams
title_full Influence of Freezing and Different Drying Methods on Volatile Profiles of Strawberry and Analysis of Volatile Compounds of Strawberry Commercial Jams
title_fullStr Influence of Freezing and Different Drying Methods on Volatile Profiles of Strawberry and Analysis of Volatile Compounds of Strawberry Commercial Jams
title_full_unstemmed Influence of Freezing and Different Drying Methods on Volatile Profiles of Strawberry and Analysis of Volatile Compounds of Strawberry Commercial Jams
title_sort influence of freezing and different drying methods on volatile profiles of strawberry and analysis of volatile compounds of strawberry commercial jams
publisher MDPI AG
series Molecules
issn 1420-3049
publishDate 2021-07-01
description Strawberry is the most consumed berry fruit worldwide due to its unique aroma and flavor. Drying fruits to produce a powder represents one of the possible conservation methods to extend their shelf-life. The aim of the present study was to compare the influence of freezing and different drying methods on the volatile profile of strawberry using the HS-SPME/GC–MS method, in addition to analysis of strawberry jam volatiles. A total of 165 compounds were identified, accounting for 85.03–96.88% of the total volatile compositions. Results and PCA showed that freezing and each drying process affected the volatile profile in a different way, and the most remarkable representative differential volatiles were ethyl hexanoate, hexyl acetate, (<i>E</i>)-2-hexenyl acetate, mesifurane, (<i>E</i>)-nerolidol, <i>γ</i>-decalactone, 1-hexanol, and acetoin. Shade air-dried, frozen, freeze-dried, and oven-dried 45 °C samples retained more of the fruity and sweet aromas of strawberry, representing more than 68% of the total aroma intensity according to the literature. In contrast, the microwave-drying method showed drastic loss of fruity esters. Strawberry jams demonstrated complete destruction of esters and alcohols in most jams, while terpenes were significantly increased. These findings help better understand the aroma of strawberry and provide a guide for the effects of drying, freezing, and jam processing.
topic strawberry
aroma
volatile organic compounds
drying methods
freezing
commercial jams
url https://www.mdpi.com/1420-3049/26/14/4153
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