Batch and Continuous Flow Preparation of Hantzsch 1,4-Dihydropyridines under Microwave Heating and Simultaneous Real-time Monitoring by Raman Spectroscopy. An Exploratory Study

Batch and Continuous Flow Preparation of Hantzsch 1,4-Dihydropyridines under Microwave Heating and Simultaneous Real-time Monitoring by Raman Spectroscopy. An Exploratory Study

Dialkyl 1,4-dihydro-2,6-dimethylpyridine-3,5-dicarboxylates have been prepared in a batch mode under conventional heating as well as under continuous flow conditions in the Miniflow 200SS, Sairem’s microwave-assisted batch and continuous flow equipment. Real-time monitoring of the reactions by Raman...

Full description

Bibliographic Details
Main Authors: Sylvain Christiaens, Xavier Vantyghem, Marilena Radoiu, Jean Jacques Vanden Eynde
Format: Article
Language:English
Published: MDPI AG 2014-07-01
Series:Molecules
Subjects:
1,4-DHPs
flow chemistry
Hantzsch pyridines
microwave
Raman spectroscopy
real-time monitoring
Online Access:http://www.mdpi.com/1420-3049/19/7/9986

Internet

http://www.mdpi.com/1420-3049/19/7/9986

Similar Items