Unusual behavior in the reactivity of 5-substituted-1H-tetrazoles in a resistively heated microreactor

The decomposition of 5-benzhydryl-1H-tetrazole in an N-methyl-2-pyrrolidone/acetic acid/water mixture was investigated under a variety of high-temperature reaction conditions. Employing a sealed Pyrex glass vial and batch microwave conditions at 240 °C, the tetrazole is comparatively stable and comp...

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Bibliographic Details
Main Authors: Bernhard Gutmann, Toma N. Glasnov, Tahseen Razzaq, Walter Goessler, Dominique M. Roberge, C. Oliver Kappe
Format: Article
Language:English
Published: Beilstein-Institut 2011-04-01
Series:Beilstein Journal of Organic Chemistry
Subjects:
Online Access:https://doi.org/10.3762/bjoc.7.59