Optimisation of the heat treatment cycles of CSIR semi-solid metal processed Al-7Si-Mg alloys A356/7

Conventional casting alloys Al-7Si-Mg A356/7 contain between 6.5 and 7.5% Si, together with 0.25-0.7% Mg and are used for critical castings in the automotive and aerospace industries. These alloys are also the most popular alloys used for semi-solid metal (SSM) forming due to good castability and fl...

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Main Author: Moller, Heinrich
Other Authors: Prof W E Stumpf
Published: 2013
Subjects:
Online Access:http://hdl.handle.net/2263/28798
Moller, H 2011, Optimisation of the heat treatment cycles of CSIR semi-solid metal processed Al-7Si-Mg alloys A356/7, PhD thesis, University of Pretoria, Pretoria, viewed yymmdd < http://hdl.handle.net/2263/28798 >
http://upetd.up.ac.za/thesis/available/etd-10172011-195355/
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spelling ndltd-netd.ac.za-oai-union.ndltd.org-up-oai-repository.up.ac.za-2263-287982017-07-20T04:11:40Z Optimisation of the heat treatment cycles of CSIR semi-solid metal processed Al-7Si-Mg alloys A356/7 Moller, Heinrich Prof W E Stumpf hmoller@up.ac.za Transmission electron microscopy High pressure die casting Rheocasting Atom probe tomography Semi-solid metal Temper Al-si-mg alloys Heat treatment Artificial aging Natural aging UCTD Conventional casting alloys Al-7Si-Mg A356/7 contain between 6.5 and 7.5% Si, together with 0.25-0.7% Mg and are used for critical castings in the automotive and aerospace industries. These alloys are also the most popular alloys used for semi-solid metal (SSM) forming due to good castability and fluidity imparted by the large volumes of the Al-Si eutectic. Despite their industrial importance, there is a lack of detailed research work revealing precipitate micro- and nanostructural evolution during aging of these alloys compared with the Al-Mg-Si 6000 series wrought alloys. This study characterises the heat treatment response of SSM-processed Al-7Si-Mg alloys in comparison with conventionally liquid cast alloys (investment casting and gravity die casting). It is shown that, provided that the maximum quantity of the alloy’s Mg is placed into solid solution during solution treatment, and that the alloy’s Fe content is within specification, the response to age hardening of Al-7Si-Mg alloys is independent of the processing technique used. The nanostructural evolution of Al- 7Si-Mg alloys after artificial aging with and without natural pre-aging has been characterized using transmission electron microscopy and atom probe tomography and correlated with hardness and mechanical tensile properties. The number densities and Mg:Si ratios of solute clusters, GP zones and β"-needles were determined. The heat treatment response of SSM-processed casting alloys A356/7 alloys are also compared with SSM-processed Al-Mg-Si 6000 series wrought alloys, with the advantage of having similar globular microstructures. The high Si-content of the casting alloys compared to the wrought alloys offers several advantages, including a faster artificial aging response (shorter T6 aging cycles), higher strength for comparable Mg contents and less sensitivity to prior natural aging on peak strength. Finally, an age-hardening model was developed for the Al-7Si-Mg alloys, including a method of incorporating the effects of changes in Mg-content on the aging curves. Thesis (PhD(Eng))--University of Pretoria, 2011. Materials Science and Metallurgical Engineering unrestricted 2013-09-07T14:15:07Z 2011-10-18 2013-09-07T14:15:07Z 2011-09-06 2011-10-18 2011-10-17 Thesis http://hdl.handle.net/2263/28798 Moller, H 2011, Optimisation of the heat treatment cycles of CSIR semi-solid metal processed Al-7Si-Mg alloys A356/7, PhD thesis, University of Pretoria, Pretoria, viewed yymmdd < http://hdl.handle.net/2263/28798 > D11/9/112/ag http://upetd.up.ac.za/thesis/available/etd-10172011-195355/ © 2011 University of Pretoria. All rights reserved. The copyright in this work vests in the University of Pretoria. No part of this work may be reproduced or transmitted in any form or by any means, without the prior written permission of the University of Pretoria.
collection NDLTD
sources NDLTD
topic Transmission electron microscopy
High pressure die casting
Rheocasting
Atom probe tomography
Semi-solid metal
Temper
Al-si-mg alloys
Heat treatment
Artificial aging
Natural aging
UCTD
spellingShingle Transmission electron microscopy
High pressure die casting
Rheocasting
Atom probe tomography
Semi-solid metal
Temper
Al-si-mg alloys
Heat treatment
Artificial aging
Natural aging
UCTD
Moller, Heinrich
Optimisation of the heat treatment cycles of CSIR semi-solid metal processed Al-7Si-Mg alloys A356/7
description Conventional casting alloys Al-7Si-Mg A356/7 contain between 6.5 and 7.5% Si, together with 0.25-0.7% Mg and are used for critical castings in the automotive and aerospace industries. These alloys are also the most popular alloys used for semi-solid metal (SSM) forming due to good castability and fluidity imparted by the large volumes of the Al-Si eutectic. Despite their industrial importance, there is a lack of detailed research work revealing precipitate micro- and nanostructural evolution during aging of these alloys compared with the Al-Mg-Si 6000 series wrought alloys. This study characterises the heat treatment response of SSM-processed Al-7Si-Mg alloys in comparison with conventionally liquid cast alloys (investment casting and gravity die casting). It is shown that, provided that the maximum quantity of the alloy’s Mg is placed into solid solution during solution treatment, and that the alloy’s Fe content is within specification, the response to age hardening of Al-7Si-Mg alloys is independent of the processing technique used. The nanostructural evolution of Al- 7Si-Mg alloys after artificial aging with and without natural pre-aging has been characterized using transmission electron microscopy and atom probe tomography and correlated with hardness and mechanical tensile properties. The number densities and Mg:Si ratios of solute clusters, GP zones and β"-needles were determined. The heat treatment response of SSM-processed casting alloys A356/7 alloys are also compared with SSM-processed Al-Mg-Si 6000 series wrought alloys, with the advantage of having similar globular microstructures. The high Si-content of the casting alloys compared to the wrought alloys offers several advantages, including a faster artificial aging response (shorter T6 aging cycles), higher strength for comparable Mg contents and less sensitivity to prior natural aging on peak strength. Finally, an age-hardening model was developed for the Al-7Si-Mg alloys, including a method of incorporating the effects of changes in Mg-content on the aging curves. === Thesis (PhD(Eng))--University of Pretoria, 2011. === Materials Science and Metallurgical Engineering === unrestricted
author2 Prof W E Stumpf
author_facet Prof W E Stumpf
Moller, Heinrich
author Moller, Heinrich
author_sort Moller, Heinrich
title Optimisation of the heat treatment cycles of CSIR semi-solid metal processed Al-7Si-Mg alloys A356/7
title_short Optimisation of the heat treatment cycles of CSIR semi-solid metal processed Al-7Si-Mg alloys A356/7
title_full Optimisation of the heat treatment cycles of CSIR semi-solid metal processed Al-7Si-Mg alloys A356/7
title_fullStr Optimisation of the heat treatment cycles of CSIR semi-solid metal processed Al-7Si-Mg alloys A356/7
title_full_unstemmed Optimisation of the heat treatment cycles of CSIR semi-solid metal processed Al-7Si-Mg alloys A356/7
title_sort optimisation of the heat treatment cycles of csir semi-solid metal processed al-7si-mg alloys a356/7
publishDate 2013
url http://hdl.handle.net/2263/28798
Moller, H 2011, Optimisation of the heat treatment cycles of CSIR semi-solid metal processed Al-7Si-Mg alloys A356/7, PhD thesis, University of Pretoria, Pretoria, viewed yymmdd < http://hdl.handle.net/2263/28798 >
http://upetd.up.ac.za/thesis/available/etd-10172011-195355/
work_keys_str_mv AT mollerheinrich optimisationoftheheattreatmentcyclesofcsirsemisolidmetalprocessedal7simgalloysa3567
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