| Summary: | 碩士 === 國立臺南大學 === 材料科學系碩士班 === 101 === In this study by use the electrospinning technique to prepared the ZnS/PVB nanofiber precursor. In the synthesis process could be prepared the thin ZnS/PVB nanofiber precursor by adjust voltage, flow rate, working distance and the PVB wt%. And finally calcination these ZnS/PVB nanofiber to synthesis ZnS nanomaterial.
Another experimental, through hydrothermal method to synthesis ZnS nanofiber by used the ZnS/PVB nanofiber precursor, in the hydrothermal process by change the reaction solvent to synthesis ZnS.
For example,1:X ( X=1-7 ) volume ratio of DI water and ethylenediamine,1:X ( X=1-7 ) volume ratio of ethylenediamine ,1:1 volume ratio of DI
water and ethylenediamine and DI water, ethylenediamine and DI water.
Finally, by using the XRD、SEM、TEM and EDX to analysis the
product of the structure and morpgology.
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