Development of chalcopyrite CuInS2 nanorods by electrospinning assisted hydrothermal process

• Main Authors: Bo-sheng Wang, 王博生
• Other Authors: Yaw-shyan Fu
• Format: Others
• Language: zh-TW
• Published: 2012
• Online Access: http://ndltd.ncl.edu.tw/handle/51513541857964045906

碩士 === 國立臺南大學 === 材料科學系碩士班 === 100 === First, this dissertation used technique of electrospinning to prepared nano-fiber materials, and explored of preparing CuInS2 the nanorod materials through the hydrothermal method.In this study, used no electrospinning method to prepared CuInS2 particles through the hydrothermal and solvothermal method. In the synthesis process, by changing different heating time and solvent to control. And discussed the change of products, viewed them as the control group.In addition, before the heat treatment.Used the simple technology of electrospinning, changing the polymer proportion, voltage, flow rate, working distance.In a suitable conditions, used technology of electrospinning to prepared the CIS/PVB nanofiber, and through subsequent heat treatment prepared CuInS2 to observe the differences of both. and by XRD, EDX, SEM, UV and TEM analysis of the structure of the product morpgology.