Syntheses and Crystal Structures of Bis-methanonaphthalimides Linked by Oligophenylene Ethers
碩士 === 國立中正大學 === 化學所 === 94 === Compounds 20, 21, and 22 are successfully synthesized from the condensation reactions of diamines 31, 32, and 33 with the anhydride 23, which is prepared from 2,3-dicyanohydroquinone in four steps: Oxidation Diels-Alder cycloaddition methylation and anhydride format...
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ndltd-TW-094CCU050650282015-10-13T10:45:18Z http://ndltd.ncl.edu.tw/handle/48945593254025049375 Syntheses and Crystal Structures of Bis-methanonaphthalimides Linked by Oligophenylene Ethers 無 Wen-I Liu 劉文毅 碩士 國立中正大學 化學所 94 Compounds 20, 21, and 22 are successfully synthesized from the condensation reactions of diamines 31, 32, and 33 with the anhydride 23, which is prepared from 2,3-dicyanohydroquinone in four steps: Oxidation Diels-Alder cycloaddition methylation and anhydride formation. By recrystallization, the single crystal of 20 grew up in the solution of toluene and acetone; and the single crystal of 21 grew up in the solution of benzene and dichloromethane; and the single crystal of 22 grew up in the solution of dichloromethane and benzene.The crystal structures of 21 and 22 are measured by X-ray crystallography. none 周德璋 2006 學位論文 ; thesis 106 zh-TW |
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碩士 === 國立中正大學 === 化學所 === 94 === Compounds 20, 21, and 22 are successfully synthesized from the condensation reactions of diamines 31, 32, and 33 with the anhydride 23, which is prepared from 2,3-dicyanohydroquinone in four steps: Oxidation Diels-Alder cycloaddition methylation and anhydride formation. By recrystallization, the single crystal of 20 grew up in the solution of toluene and acetone; and the single crystal of 21 grew up in the solution of benzene and dichloromethane; and the single crystal of 22 grew up in the solution of dichloromethane and benzene.The crystal structures of 21 and 22 are measured by X-ray crystallography.
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none Wen-I Liu 劉文毅 |
author |
Wen-I Liu 劉文毅 |
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Wen-I Liu 劉文毅 Syntheses and Crystal Structures of Bis-methanonaphthalimides Linked by Oligophenylene Ethers |
author_sort |
Wen-I Liu |
title |
Syntheses and Crystal Structures of Bis-methanonaphthalimides Linked by Oligophenylene Ethers |
title_short |
Syntheses and Crystal Structures of Bis-methanonaphthalimides Linked by Oligophenylene Ethers |
title_full |
Syntheses and Crystal Structures of Bis-methanonaphthalimides Linked by Oligophenylene Ethers |
title_fullStr |
Syntheses and Crystal Structures of Bis-methanonaphthalimides Linked by Oligophenylene Ethers |
title_full_unstemmed |
Syntheses and Crystal Structures of Bis-methanonaphthalimides Linked by Oligophenylene Ethers |
title_sort |
syntheses and crystal structures of bis-methanonaphthalimides linked by oligophenylene ethers |
publishDate |
2006 |
url |
http://ndltd.ncl.edu.tw/handle/48945593254025049375 |
work_keys_str_mv |
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1716832869774524416 |