Thermally Safe Operation of a Conventional Batch Reactor: Experimental Study

• Main Authors: Jr-BinYang, 楊智斌
• Other Authors: Jyh-Shyong Chang
• Format: Others
• Language: en_US
• Published: 1999
• Online Access: http://ndltd.ncl.edu.tw/handle/05411026915910302999

碩士 === 大同大學 === 化學工程研究所 === 88 === In this work, we proposed the way to determine safe operation trajectories based on the identified physical and identified hybrid model. Operational temperature trajectories were calculated to meet the thermally safe operation criterion in case of known or unknown reaction kinetics. The proposed method was examined in a 10-L conventional batch reactor in which a highly exothermic hydrolysis reaction of the acetic anhydride occurred with or without sulfuric acid as catalyst. Experimental demonstrations were successful, and the suggested approach can be applied in the industrial conditions especially the hybrid model approach.