The Device and Data Analysis of Susceptibility Measurement

碩士 === 淡江大學 === 物理學系 === 86 === Ac magnetic susceptibility measurements are widely used for sample characterization in material study . Since the magnetic properties of the entire sample can be revealed in the measurements , it is very impo...

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Bibliographic Details
Main Authors: Wu, HSIAO-PING, 吳曉蘋
Other Authors: Chien Fan-Z
Format: Others
Language:zh-TW
Published: 1998
Online Access:http://ndltd.ncl.edu.tw/handle/17923205204596413692
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Summary:碩士 === 淡江大學 === 物理學系 === 86 === Ac magnetic susceptibility measurements are widely used for sample characterization in material study . Since the magnetic properties of the entire sample can be revealed in the measurements , it is very important for superconducting studies. The ac susceptibility measuring system includes a CRYOSTAT and a coil detection device . The coil detection device consists of a primary coil and secondary coils . Primary coil supplies an ac magnetic field H which would induce magnetization in the sample . It will then result in a signal of the secondary coils given by χac = dM / dH . Therefore the temperature dependent χac can be determined. Unsatisfactory results were obtained in using our ac magnetic susceptibility system bought from U.S.A. . Many defects were found. For example, (1) the accuracy of χac is not acceptable , (2) the arrangement of the temperature sensor need to be readjusted , (3) each measurement takesup to 10 hours, (4) the lowest working temperature of the system is 39K . A new design for CRYOSTAT has been carried out since most of the defects were found to be due to the improper design of original CRYOSTAT. The previous problems have been improved. Satisfactory results have been achieved and demonstrated in a series of measurements.