The Study of Activated Carbon From Sugar

碩士 === 逢甲大學 === 材料科學研究所 === 85 === ABSTRACT In this study, we try to use sugar as the precursor to activated carbon. The experiment includes the action of precursor at carbonization (heat treatment temperature ranging from 600 to 1...

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Main Authors: Su, Cheng-Lin, 蘇宗麟
Other Authors: Tse-Hao Ko
Format: Others
Language:zh-TW
Published: 1997
Online Access:http://ndltd.ncl.edu.tw/handle/25666700301066135210
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spelling ndltd-TW-085FCU001590042015-10-13T12:15:15Z http://ndltd.ncl.edu.tw/handle/25666700301066135210 The Study of Activated Carbon From Sugar 以黑糖製造活性碳之研究 Su, Cheng-Lin 蘇宗麟 碩士 逢甲大學 材料科學研究所 85 ABSTRACT In this study, we try to use sugar as the precursor to activated carbon. The experiment includes the action of precursor at carbonization (heat treatment temperature ranging from 600 to 1000℃),and also the behavior of precursor within carbonization and activation in one step (activated steam 0.50~1.00 min for 10min at each temperatures ).In-order to find out the effect of sugarthe physical properties and microstructure, the microstructure was investigated by element analysis、X-ray diffraction、Raman laser scattering and SEM. The analysis of physical properties were carried out with density、 weight loss. Besides, the effect of activations on porosity of carbon was characterized by nitrogen adsorption and desorption at 77K, the N2 surface area and pore size distribution were calculated by using the BET equation and the procedure developed by Barrett et al[1]. When heat treatment temperature (HTT) raised, there is a increasing tendency of weight loss and density of the samples, it also found at the surface are a lot of porous structure by SEM observation, and the amount of pores increase as the treatment steam increases. From X-ray and Raman laser scattering analysis, we found that molecule H2O can penetrate into the carbon, it would led to connect the internal and exteroal pore systems in samples, the stacking (Lc)decrease and the length (La) of carbon layers were suudied as a function of both temperature and steam pyrolysis. On the other hand, the distribution of pores are mainly mesopores,the activated carbon produced with steam pyrolysis have the highest specific surface area of 688.8 (m2/g).Within the studies of sugar, we found it is feasible to be an adsorbent. Tse-Hao Ko 柯澤豪 1997 學位論文 ; thesis 4 zh-TW
collection NDLTD
language zh-TW
format Others
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description 碩士 === 逢甲大學 === 材料科學研究所 === 85 === ABSTRACT In this study, we try to use sugar as the precursor to activated carbon. The experiment includes the action of precursor at carbonization (heat treatment temperature ranging from 600 to 1000℃),and also the behavior of precursor within carbonization and activation in one step (activated steam 0.50~1.00 min for 10min at each temperatures ).In-order to find out the effect of sugarthe physical properties and microstructure, the microstructure was investigated by element analysis、X-ray diffraction、Raman laser scattering and SEM. The analysis of physical properties were carried out with density、 weight loss. Besides, the effect of activations on porosity of carbon was characterized by nitrogen adsorption and desorption at 77K, the N2 surface area and pore size distribution were calculated by using the BET equation and the procedure developed by Barrett et al[1]. When heat treatment temperature (HTT) raised, there is a increasing tendency of weight loss and density of the samples, it also found at the surface are a lot of porous structure by SEM observation, and the amount of pores increase as the treatment steam increases. From X-ray and Raman laser scattering analysis, we found that molecule H2O can penetrate into the carbon, it would led to connect the internal and exteroal pore systems in samples, the stacking (Lc)decrease and the length (La) of carbon layers were suudied as a function of both temperature and steam pyrolysis. On the other hand, the distribution of pores are mainly mesopores,the activated carbon produced with steam pyrolysis have the highest specific surface area of 688.8 (m2/g).Within the studies of sugar, we found it is feasible to be an adsorbent.
author2 Tse-Hao Ko
author_facet Tse-Hao Ko
Su, Cheng-Lin
蘇宗麟
author Su, Cheng-Lin
蘇宗麟
spellingShingle Su, Cheng-Lin
蘇宗麟
The Study of Activated Carbon From Sugar
author_sort Su, Cheng-Lin
title The Study of Activated Carbon From Sugar
title_short The Study of Activated Carbon From Sugar
title_full The Study of Activated Carbon From Sugar
title_fullStr The Study of Activated Carbon From Sugar
title_full_unstemmed The Study of Activated Carbon From Sugar
title_sort study of activated carbon from sugar
publishDate 1997
url http://ndltd.ncl.edu.tw/handle/25666700301066135210
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