Synthesis and Characterization of 1,1-Di-Tert-Butyldiazene

Synthesis and Characterization of 1,1-Di-Tert-Butyldiazene

<p>The synthesis and direct observation of 1,1-di-tert-butyldiazene (16) at -127°C is described. The absorption spectrum of a red solution of 1,1-diazene 16 reveals a structured absorption band with λ<sub>max</sub> at 506 nm (Me<sub>2</sub>O, -125°C). The vibrational sp...

Full description

Bibliographic Details
Main Author:	McIntyre, Daniel Keith
Format:	Others
Language:	en
Published:	1983
Online Access:	https://thesis.library.caltech.edu/8035/2/McIntyre%201983.pdf McIntyre, Daniel Keith (1983) Synthesis and Characterization of 1,1-Di-Tert-Butyldiazene. Dissertation (Ph.D.), California Institute of Technology. doi:10.7907/y54d-s069. https://resolver.caltech.edu/CaltechTHESIS:12022013-142422017 <https://resolver.caltech.edu/CaltechTHESIS:12022013-142422017>

Similar Items

Di-tert-butyl 2-benzoylhydrazine-1,1-dicarboxylate
by: Claude Didierjean, et al.
Published: (2008-01-01)

The Stereochemistry of 1,4-Di-Tert-Butyl-1,4-Dihydronaphthalene
by: McDaniel, Oya A.
Published: (1980)

(R)-Di-tert-butyl 1,1′-binaphthyl-2,2′-dicarboxylate
by: Martin Feigel, et al.
Published: (2009-02-01)

1,1&#8242;-Bis(tert-butyldimethylsilyl)ferrocene
by: Abdolreza Abri, et al.
Published: (2013-01-01)

1,1′-Methylenebis(4-tert-butylpyridinium) dichloride hemihydrate
by: J.P.J. Bruekers, et al.
Published: (2021-08-01)

1,2-Di-tert-butylethane-1,2-diyl bis(tert-butanesulfinamide)
by: Xiaoxia Sun, et al.
Published: (2009-01-01)

Synthesis and Reactivity Studies of 1,3-di-tert-butylcyclopentadienylcopper Complexes
by: Chang, Hao-Chieh, et al.
Published: (2018)

Di-tert-butyl (1,1&#8242;-binaphthyl-2,2&#8242;-dioxy)diacetate
by: Asra Mustafa, et al.
Published: (2009-04-01)

(1S*,2S*)-1,2-Di-tert-butylglycol
by: Tobias Kerscher, et al.
Published: (2009-01-01)

3,3&#8242;-Di-tert-butyl-1,1&#8242;-[1,3-phenylenebis(methylene)]diurea
by: Md. Alamgir Hossain, et al.
Published: (2010-03-01)

1,8-bis(2-hydroxy-3,5-di-tert-butylbenzyl)-4,11-dibenzyl-1,4,8,11-tetraazacyclotetradecane
by: Ane I. Aranburu Leiva, et al.
Published: (2017-10-01)

2,2,2-Trichloro-1,1-dimethylethyl 4-tert-butylbenzoate
by: Éva Klement, et al.
Published: (2004-03-01)

1,1&#8242;-Bis[bis(4-tert-butylphenyl)methyl]ferrocene
by: Heiko Bauer, et al.
Published: (2012-12-01)

Studies on the Thermal Decomposition and Incompatible Reaction of 1,1-Bis(tert-butylperoxy)Cyclohexane
by: Kuang-Hua Hsueh, et al.
Published: (2015)

1-Bromo-2,7-di-tert-butylpyrene
by: Guang-Ming Xia, et al.
Published: (2010-01-01)

Synthesis, Neuroprotection, and Antioxidant Activity of 1,1′-Biphenylnitrones as α-Phenyl-<i>N-tert</i>-Butylnitrone Analogues in In Vitro Ischemia Models
by: Beatriz Chamorro, et al.
Published: (2021-02-01)

Synthesis and Characterization of Group-13-Bridged [1]- and [1.1]Metallacyclophanes
by: Lund, Clinton Laine
Published: (2008)

(3,5-Di-tert-butyl-2-ethoxybenzylidene)[2-(3,5-di-tert-butyl-1H-pyrazol-1-yl)ethyl]amine
by: Lara C. Spencer, et al.
Published: (2012-08-01)

Di-tert-butyl 2,6,11-trioxo-2,3-dihydro-1H-anthra[1,2-d]imidazole-1,3-diacetate
by: Zahra Afrakssou, et al.
Published: (2011-07-01)

Synthesis , Characterization and Electronichemical of 1,1-Diferrocenyl Disulfide compounds
by: Tseng,Jiung Fu, et al.
Published: (1995)

<i>tert</i>-Butyl Bis(4′-(Hexyloxy)-[1,1′-biphenyl]-4-yl)carbamate
by: Timofey N. Chmovzh, et al.
Published: (2021-07-01)

Bis[(1,1&#8242;-biphenyl-2,2&#8242;-diyl)di-tert-butylphosphonium] di-&#956;-chlorido-bis[dichloridopalladate(II)]
by: Charmaine Arderne, et al.
Published: (2012-10-01)

Synthesis and Molecular Structure of tert-Butyl 4-(2-tert-butoxy-2-oxoethyl)piperazine-1-carboxylate
by: Martin Köckerling, et al.
Published: (2012-02-01)

Synthesis and Characterization of Nickel and Zinc Metal Complexes Containing Bis(3,6-di-tert-butyl-1(imidazolium-1-yl) carbazolide)-xylene Derivatives as Ligands
by: KUO, LIANG-YEN, et al.
Published: (2018)

4-tert-Butylpyridinium triiodide&#8211;4-tert-butylpyridine (1/1)
by: Hongshan He, et al.
Published: (2011-02-01)

1-(4-tert-Butylbenzyl)-2-(4-tert-butylphenyl)-1H-benzimidazole
by: Chuan-Ming Zhang, et al.
Published: (2009-12-01)

Di-tert-butyl 3,3&#8242;-(2,2&#8242;-bi-1H-imidazole-1,1&#8242;-diyl)dipropanoate
by: Ke Wang, et al.
Published: (2009-07-01)

Difunctionalization of alkenes with iodine and tert-butyl hydroperoxide (TBHP) at room temperature for the synthesis of 1-(tert-butylperoxy)-2-iodoethanes
by: Hao Wang, et al.
Published: (2017-09-01)

Electron Transfer-Induced Coupling of Haloarenes to Styrenes and 1,1-Diphenylethenes Triggered by Diketopiperazines and Potassium tert-Butoxide
by: Eswararao Doni, et al.
Published: (2015-01-01)

2,4-Di-tert-butyl-6-[1-(3,5-di-tert-butyl-2-hydroxyphenyl)ethyl]phenyl 4-methylbenzenesulfonate
by: Jincai Wu, et al.
Published: (2009-01-01)

Synthesis and Characterization of Soluble Polyamide-imides with tert-butyl group
by: Meng-Hsiung Su, et al.
Published: (2002)

The study of the thermal decomposition of Tetracyclo[3.3.1.1[sup 3,7].0[sup 1,3]]decane in octane and cumene at 1950
by: McIntyre, Brian William
Published: (2010)

Effects of the environment on the conformational stability of the chloride intracellular channel protein CLIC1
by: McIntyre, Sylvia
Published: (2008)

1,1&#8242;-Di-tert-butyl-2,2&#8242;,3,3&#8242;,4,4&#8242;,5,5&#8242;-octaethyl-1,1&#8242;-bistannole
by: Takuya Kuwabara, et al.
Published: (2011-07-01)

(E)-2&#8242;-[(3,5-Di-tert-butyl-2-hydroxybenzylidene)amino]-1,1&#8242;-binaphthalen-2-ol methanol monosolvate
by: Dian He, et al.
Published: (2011-11-01)

3,5-Di-tert-butyl-1H-pyrazole-4-carbonitrile
by: Ningfeng Zhao, et al.
Published: (2016-04-01)

Di-tert-butyl cyclohex-2-ene-1,4-diyl dicarbonate
by: Syed Nawazish Ali, et al.
Published: (2009-11-01)

Crystal structure of 1,5-di-tert-butyl-2-iminoimidazolidin-4-one, C11H21N3O
by: Reibenspies J. H., et al.
Published: (1998-04-01)

The role of integrin a7B1 in skeletal muscle differentiation and signalling
by: McIntyre, Jennifer
Published: (2009)

Synthesis of Surfactant Tert-Butyl Glycosides from Glucose and Tert-Butanol
by: Harsa Pawignya, et al.
Published: (2019-03-01)