1D and 2D NMR studies of BENZYL O-VANILLIN

1D and 2D NMR studies of BENZYL O-VANILLIN

The reaction of o-vanillin A with benzyl bromide B2 in acetone as the solvent and K2CO3 as a base in the presence of tetra-n-butylammonium iodide (TBAI) as catalyst formed benzyl o-vanillin, C. The complete assignments of C using PROTON, APT, DEPT-135, COSY, NOESY, HMQC and HMBC NMR in both CDCl3 an...

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Bibliographic Details
Main Authors: Al-Douh, Mohammed Hadi (Author), Abdul Hamid, Shafida (Author), Osman, Hasnah (Author)
Format: Article
Language:English
Published: Universitas Gadjah Mada, 2008.
Subjects:
QD1-999 Chemistry
Online Access:Get fulltext
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042 |a dc 
100 1 0 |a Al-Douh, Mohammed Hadi  |e author 
700 1 0 |a Abdul Hamid, Shafida   |e author 
700 1 0 |a Osman, Hasnah   |e author 
245 0 0 |a 1D and 2D NMR studies of BENZYL O-VANILLIN 
260 |b Universitas Gadjah Mada,   |c 2008. 
856 |z Get fulltext  |u http://eprints.usm.my/37938/1/1D_AND_2D_NMR_STUDIES_OF_BENZYL_O%E2%80%93VANILLIN.pdf 
520 |a The reaction of o-vanillin A with benzyl bromide B2 in acetone as the solvent and K2CO3 as a base in the presence of tetra-n-butylammonium iodide (TBAI) as catalyst formed benzyl o-vanillin, C. The complete assignments of C using PROTON, APT, DEPT-135, COSY, NOESY, HMQC and HMBC NMR in both CDCl3 and acetone-d6 are discussed, and the coupling constants J are reported in Hertz (Hz). 
546 |a en 
650 0 4 |a QD1-999 Chemistry 

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