Metal Acetylacetonates as General Precursors for the Synthesis of Early Transition Metal Oxide Nanomaterials

Metal Acetylacetonates as General Precursors for the Synthesis of Early Transition Metal Oxide Nanomaterials

A versatile, convenient, and nontoxic solvothermal method for the synthesis of nanocrystalline iron, chromium, and manganese oxides is described. This method employs the reactions of metal acetylacetonate precursors and oxygen-containing solvents in a reaction to prepare metal oxide nanoparticles. C...

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Main Authors: Amanda L. Willis, Zhuoying Chen, Jiaqing He, Yimei Zhu, Nicholas J. Turro, Stephen O'Brien
Format: Article
Language:English
Published: Hindawi Limited 2007-01-01
Series:Journal of Nanomaterials
Online Access:http://dx.doi.org/10.1155/2007/14858
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spelling doaj-fb58f40f6c1541bf86fb708acf1e200a2020-11-25T01:20:39ZengHindawi LimitedJournal of Nanomaterials1687-41101687-41292007-01-01200710.1155/2007/1485814858Metal Acetylacetonates as General Precursors for the Synthesis of Early Transition Metal Oxide NanomaterialsAmanda L. Willis0Zhuoying Chen1Jiaqing He2Yimei Zhu3Nicholas J. Turro4Stephen O'Brien5Department of Chemistry, Columbia University, New York, NY 10027, USADepartment of Applied Physics and Applied Mathematics, Columbia University, New York, NY 10027, USADepartment of Materials Science, Brookhaven National Lab, Upton, NY 11973, USADepartment of Materials Science, Brookhaven National Lab, Upton, NY 11973, USADepartment of Chemistry, Columbia University, New York, NY 10027, USADepartment of Applied Physics and Applied Mathematics, Columbia University, New York, NY 10027, USAA versatile, convenient, and nontoxic solvothermal method for the synthesis of nanocrystalline iron, chromium, and manganese oxides is described. This method employs the reactions of metal acetylacetonate precursors and oxygen-containing solvents in a reaction to prepare metal oxide nanoparticles. Characterization of these nanocrystalline materials was carried out employing transmission electron microscopy (TEM), high-resolution TEM (HRTEM), X-ray diffraction (XRD), and elemental analysis.http://dx.doi.org/10.1155/2007/14858
collection DOAJ
language English
format Article
sources DOAJ
author Amanda L. Willis
Zhuoying Chen
Jiaqing He
Yimei Zhu
Nicholas J. Turro
Stephen O'Brien
spellingShingle Amanda L. Willis
Zhuoying Chen
Jiaqing He
Yimei Zhu
Nicholas J. Turro
Stephen O'Brien
Metal Acetylacetonates as General Precursors for the Synthesis of Early Transition Metal Oxide Nanomaterials
Journal of Nanomaterials
author_facet Amanda L. Willis
Zhuoying Chen
Jiaqing He
Yimei Zhu
Nicholas J. Turro
Stephen O'Brien
author_sort Amanda L. Willis
title Metal Acetylacetonates as General Precursors for the Synthesis of Early Transition Metal Oxide Nanomaterials
title_short Metal Acetylacetonates as General Precursors for the Synthesis of Early Transition Metal Oxide Nanomaterials
title_full Metal Acetylacetonates as General Precursors for the Synthesis of Early Transition Metal Oxide Nanomaterials
title_fullStr Metal Acetylacetonates as General Precursors for the Synthesis of Early Transition Metal Oxide Nanomaterials
title_full_unstemmed Metal Acetylacetonates as General Precursors for the Synthesis of Early Transition Metal Oxide Nanomaterials
title_sort metal acetylacetonates as general precursors for the synthesis of early transition metal oxide nanomaterials
publisher Hindawi Limited
series Journal of Nanomaterials
issn 1687-4110
1687-4129
publishDate 2007-01-01
description A versatile, convenient, and nontoxic solvothermal method for the synthesis of nanocrystalline iron, chromium, and manganese oxides is described. This method employs the reactions of metal acetylacetonate precursors and oxygen-containing solvents in a reaction to prepare metal oxide nanoparticles. Characterization of these nanocrystalline materials was carried out employing transmission electron microscopy (TEM), high-resolution TEM (HRTEM), X-ray diffraction (XRD), and elemental analysis.
url http://dx.doi.org/10.1155/2007/14858
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AT zhuoyingchen metalacetylacetonatesasgeneralprecursorsforthesynthesisofearlytransitionmetaloxidenanomaterials
AT jiaqinghe metalacetylacetonatesasgeneralprecursorsforthesynthesisofearlytransitionmetaloxidenanomaterials
AT yimeizhu metalacetylacetonatesasgeneralprecursorsforthesynthesisofearlytransitionmetaloxidenanomaterials
AT nicholasjturro metalacetylacetonatesasgeneralprecursorsforthesynthesisofearlytransitionmetaloxidenanomaterials
AT stephenobrien metalacetylacetonatesasgeneralprecursorsforthesynthesisofearlytransitionmetaloxidenanomaterials
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