Crystal structure of 2-[9-(2-hydroxyphenyl)-1,8-dioxo-1,2,3,4,5,6,7,8,9,10-decahydroacridin-10-yl]acetic acid

Crystal structure of 2-[9-(2-hydroxyphenyl)-1,8-dioxo-1,2,3,4,5,6,7,8,9,10-decahydroacridin-10-yl]acetic acid

The title compound, C21H21NO5, crystallizes with two molecules in the asymmetric unit. In each molecule, the central 1,4-dihydropyridine ring adopts a shallow sofa conformations (with the C atom bearing the phenol ring as the flap), whereas the pendant cyclohexene rings both have twisted-boat confor...

Full description

Bibliographic Details
Main Authors: Mehmet Akkurt, Jerry P. Jasinski, Shaaban K. Mohamed, Omyma A. Abd Allah, Asmaa H. A. Tamam, Mustafa R. Albayati
Format: Article
Language:English
Published: International Union of Crystallography 2015-12-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
crystal structure
acridines
acetic acid
hydrogen bonding
C—H...π interactions
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989015021611
id doaj-fb45e7587d864e788be457280ea79bc5
record_format Article
spelling doaj-fb45e7587d864e788be457280ea79bc52020-11-25T00:59:06ZengInternational Union of CrystallographyActa Crystallographica Section E: Crystallographic Communications2056-98902015-12-017112o963o96410.1107/S2056989015021611hb7542Crystal structure of 2-[9-(2-hydroxyphenyl)-1,8-dioxo-1,2,3,4,5,6,7,8,9,10-decahydroacridin-10-yl]acetic acidMehmet Akkurt0Jerry P. Jasinski1Shaaban K. Mohamed2Omyma A. Abd Allah3Asmaa H. A. Tamam4Mustafa R. Albayati5Department of Physics, Faculty of Sciences, Erciyes University, 38039 Kayseri, TurkeyDepartment of Chemistry, Keene State College, 229 Main Street, Keene, NH 03435-2001, USAChemistry and Environmental Division, Manchester Metropolitan University, Manchester M1 5GD, EnglandChemistry Department, Faculty of Science, Sohag University, 82524 Sohag, EgyptChemistry Department, Faculty of Science, Sohag University, 82524 Sohag, EgyptKirkuk University, College of Science, Department of Chemistry, Kirkuk, IraqThe title compound, C21H21NO5, crystallizes with two molecules in the asymmetric unit. In each molecule, the central 1,4-dihydropyridine ring adopts a shallow sofa conformations (with the C atom bearing the phenol ring as the flap), whereas the pendant cyclohexene rings both have twisted-boat conformations. Each molecule features an intramolecular O—H...O hydrogen bond, which closes an S(8) ring. In the crystal, the molecules are linked by O—H...O, C—H...O and C—H...π interactions, forming a three-dimensional network.http://scripts.iucr.org/cgi-bin/paper?S2056989015021611crystal structureacridinesacetic acidhydrogen bondingC—H...π interactions
collection DOAJ
language English
format Article
sources DOAJ
author Mehmet Akkurt
Jerry P. Jasinski
Shaaban K. Mohamed
Omyma A. Abd Allah
Asmaa H. A. Tamam
Mustafa R. Albayati
spellingShingle Mehmet Akkurt
Jerry P. Jasinski
Shaaban K. Mohamed
Omyma A. Abd Allah
Asmaa H. A. Tamam
Mustafa R. Albayati
Crystal structure of 2-[9-(2-hydroxyphenyl)-1,8-dioxo-1,2,3,4,5,6,7,8,9,10-decahydroacridin-10-yl]acetic acid
Acta Crystallographica Section E: Crystallographic Communications
crystal structure
acridines
acetic acid
hydrogen bonding
C—H...π interactions
author_facet Mehmet Akkurt
Jerry P. Jasinski
Shaaban K. Mohamed
Omyma A. Abd Allah
Asmaa H. A. Tamam
Mustafa R. Albayati
author_sort Mehmet Akkurt
title Crystal structure of 2-[9-(2-hydroxyphenyl)-1,8-dioxo-1,2,3,4,5,6,7,8,9,10-decahydroacridin-10-yl]acetic acid
title_short Crystal structure of 2-[9-(2-hydroxyphenyl)-1,8-dioxo-1,2,3,4,5,6,7,8,9,10-decahydroacridin-10-yl]acetic acid
title_full Crystal structure of 2-[9-(2-hydroxyphenyl)-1,8-dioxo-1,2,3,4,5,6,7,8,9,10-decahydroacridin-10-yl]acetic acid
title_fullStr Crystal structure of 2-[9-(2-hydroxyphenyl)-1,8-dioxo-1,2,3,4,5,6,7,8,9,10-decahydroacridin-10-yl]acetic acid
title_full_unstemmed Crystal structure of 2-[9-(2-hydroxyphenyl)-1,8-dioxo-1,2,3,4,5,6,7,8,9,10-decahydroacridin-10-yl]acetic acid
title_sort crystal structure of 2-[9-(2-hydroxyphenyl)-1,8-dioxo-1,2,3,4,5,6,7,8,9,10-decahydroacridin-10-yl]acetic acid
publisher International Union of Crystallography
series Acta Crystallographica Section E: Crystallographic Communications
issn 2056-9890
publishDate 2015-12-01
description The title compound, C21H21NO5, crystallizes with two molecules in the asymmetric unit. In each molecule, the central 1,4-dihydropyridine ring adopts a shallow sofa conformations (with the C atom bearing the phenol ring as the flap), whereas the pendant cyclohexene rings both have twisted-boat conformations. Each molecule features an intramolecular O—H...O hydrogen bond, which closes an S(8) ring. In the crystal, the molecules are linked by O—H...O, C—H...O and C—H...π interactions, forming a three-dimensional network.
topic crystal structure
acridines
acetic acid
hydrogen bonding
C—H...π interactions
url http://scripts.iucr.org/cgi-bin/paper?S2056989015021611
work_keys_str_mv AT mehmetakkurt crystalstructureof292hydroxyphenyl18dioxo12345678910decahydroacridin10ylaceticacid
AT jerrypjasinski crystalstructureof292hydroxyphenyl18dioxo12345678910decahydroacridin10ylaceticacid
AT shaabankmohamed crystalstructureof292hydroxyphenyl18dioxo12345678910decahydroacridin10ylaceticacid
AT omymaaabdallah crystalstructureof292hydroxyphenyl18dioxo12345678910decahydroacridin10ylaceticacid
AT asmaahatamam crystalstructureof292hydroxyphenyl18dioxo12345678910decahydroacridin10ylaceticacid
AT mustafaralbayati crystalstructureof292hydroxyphenyl18dioxo12345678910decahydroacridin10ylaceticacid
_version_ 1725218846101471232

Similar Items