N-(5-Sulfanylidene-4,5-dihydro-1,3,4-thiadiazol-2-yl)acetamide dimethyl sulfoxide disolvate

N-(5-Sulfanylidene-4,5-dihydro-1,3,4-thiadiazol-2-yl)acetamide dimethyl sulfoxide disolvate

In the title compound, C4H5N3OS2·2C2H6OS, the five-membered heterocyclic ring and the N—(C=O)—C plane of the acetamide group are essentially co-planar, with a dihedral angle of 1.25 (3)°. Intermolecular N—H...O hydroge...

Full description

Bibliographic Details
Main Authors: Sung Kwon Kang, Nam Sook Cho, Siyoung Jang
Format: Article
Language:English
Published: International Union of Crystallography 2012-01-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536811054298
id doaj-faacd84cfc3d496abf0a3805c0de6dc0
record_format Article
spelling doaj-faacd84cfc3d496abf0a3805c0de6dc02020-11-25T00:12:32ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682012-01-01681o224o22410.1107/S1600536811054298N-(5-Sulfanylidene-4,5-dihydro-1,3,4-thiadiazol-2-yl)acetamide dimethyl sulfoxide disolvateSung Kwon KangNam Sook ChoSiyoung JangIn the title compound, C4H5N3OS2·2C2H6OS, the five-membered heterocyclic ring and the N—(C=O)—C plane of the acetamide group are essentially co-planar, with a dihedral angle of 1.25 (3)°. Intermolecular N—H...O hydrogen bonds between the acetamide compound and the dimethyl sulfoxide molecules stabilize the crystal structure. The two dimethyl sulfoxide molecules are each disordered over two positions with occupancy ratios of 0.605 (2):0.395 (2) and 0.8629 (18):0.1371 (18).http://scripts.iucr.org/cgi-bin/paper?S1600536811054298
collection DOAJ
language English
format Article
sources DOAJ
author Sung Kwon Kang
Nam Sook Cho
Siyoung Jang
spellingShingle Sung Kwon Kang
Nam Sook Cho
Siyoung Jang
N-(5-Sulfanylidene-4,5-dihydro-1,3,4-thiadiazol-2-yl)acetamide dimethyl sulfoxide disolvate
Acta Crystallographica Section E
author_facet Sung Kwon Kang
Nam Sook Cho
Siyoung Jang
author_sort Sung Kwon Kang
title N-(5-Sulfanylidene-4,5-dihydro-1,3,4-thiadiazol-2-yl)acetamide dimethyl sulfoxide disolvate
title_short N-(5-Sulfanylidene-4,5-dihydro-1,3,4-thiadiazol-2-yl)acetamide dimethyl sulfoxide disolvate
title_full N-(5-Sulfanylidene-4,5-dihydro-1,3,4-thiadiazol-2-yl)acetamide dimethyl sulfoxide disolvate
title_fullStr N-(5-Sulfanylidene-4,5-dihydro-1,3,4-thiadiazol-2-yl)acetamide dimethyl sulfoxide disolvate
title_full_unstemmed N-(5-Sulfanylidene-4,5-dihydro-1,3,4-thiadiazol-2-yl)acetamide dimethyl sulfoxide disolvate
title_sort n-(5-sulfanylidene-4,5-dihydro-1,3,4-thiadiazol-2-yl)acetamide dimethyl sulfoxide disolvate
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2012-01-01
description In the title compound, C4H5N3OS2·2C2H6OS, the five-membered heterocyclic ring and the N—(C=O)—C plane of the acetamide group are essentially co-planar, with a dihedral angle of 1.25 (3)°. Intermolecular N—H...O hydrogen bonds between the acetamide compound and the dimethyl sulfoxide molecules stabilize the crystal structure. The two dimethyl sulfoxide molecules are each disordered over two positions with occupancy ratios of 0.605 (2):0.395 (2) and 0.8629 (18):0.1371 (18).
url http://scripts.iucr.org/cgi-bin/paper?S1600536811054298
work_keys_str_mv AT sungkwonkang n5sulfanylidene45dihydro134thiadiazol2ylacetamidedimethylsulfoxidedisolvate
AT namsookcho n5sulfanylidene45dihydro134thiadiazol2ylacetamidedimethylsulfoxidedisolvate
AT siyoungjang n5sulfanylidene45dihydro134thiadiazol2ylacetamidedimethylsulfoxidedisolvate
_version_ 1725399034401652736

Similar Items