Determination of Susceptibility to Intergranular Corrosion of UNS 31803 Type Duplex Stainless Steel by Electrochemical Reactivation Method: A Comparative Study

In the present study as in our previous studies (Arikan and Doruk, 2008 and Arikan et al., 2012), similar specimens taken from a hot rolled cylindrical duplex stainless steel (DSS) bar with 22% Cr grade were solution annealed at 1050°C and then aged at 800∘C from 100 to 31622 min for sensitization t...

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Main Authors: Mehmet Emin Arıkan, Rafet Arıkan, Mustafa Doruk
Format: Article
Language:English
Published: Hindawi Limited 2012-01-01
Series:International Journal of Corrosion
Online Access:http://dx.doi.org/10.1155/2012/478508
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spelling doaj-f6c530578c8e471f9fe1eba4ca6a51e52020-11-24T20:52:57ZengHindawi LimitedInternational Journal of Corrosion1687-93251687-93332012-01-01201210.1155/2012/478508478508Determination of Susceptibility to Intergranular Corrosion of UNS 31803 Type Duplex Stainless Steel by Electrochemical Reactivation Method: A Comparative StudyMehmet Emin Arıkan0Rafet Arıkan1Mustafa Doruk2Metallurgical and Materials Engineering Department, METU, 06800 Çankaya, Ankara, TurkeyMechanical Engineering Department, Faculty of Engineering, Atılım University, 06836 Incek, Ankara, TurkeyMetallurgical and Materials Engineering Department, METU, 06800 Çankaya, Ankara, TurkeyIn the present study as in our previous studies (Arikan and Doruk, 2008 and Arikan et al., 2012), similar specimens taken from a hot rolled cylindrical duplex stainless steel (DSS) bar with 22% Cr grade were solution annealed at 1050°C and then aged at 800∘C from 100 to 31622 min for sensitization treatment. Double loop electrochemical potentiodynamic reactivation and standard weight loss immersion acid tests were conducted. The solution annealed samples were found unsensitized. The samples aged for 100 min were less sensitized whereas samples aged for 316 min and more time were sensitized. The degree of sensitization (DOS) can be attributed to higher contribution of chromium and molybdenum depleted areas that result from intermetallic phases. However, especially the samples aged from 3162 to 31622 min have revealed chromium replenishment. Consequently, the degree of sensitization was lowered in comparison to the results obtained in previous studies.http://dx.doi.org/10.1155/2012/478508
collection DOAJ
language English
format Article
sources DOAJ
author Mehmet Emin Arıkan
Rafet Arıkan
Mustafa Doruk
spellingShingle Mehmet Emin Arıkan
Rafet Arıkan
Mustafa Doruk
Determination of Susceptibility to Intergranular Corrosion of UNS 31803 Type Duplex Stainless Steel by Electrochemical Reactivation Method: A Comparative Study
International Journal of Corrosion
author_facet Mehmet Emin Arıkan
Rafet Arıkan
Mustafa Doruk
author_sort Mehmet Emin Arıkan
title Determination of Susceptibility to Intergranular Corrosion of UNS 31803 Type Duplex Stainless Steel by Electrochemical Reactivation Method: A Comparative Study
title_short Determination of Susceptibility to Intergranular Corrosion of UNS 31803 Type Duplex Stainless Steel by Electrochemical Reactivation Method: A Comparative Study
title_full Determination of Susceptibility to Intergranular Corrosion of UNS 31803 Type Duplex Stainless Steel by Electrochemical Reactivation Method: A Comparative Study
title_fullStr Determination of Susceptibility to Intergranular Corrosion of UNS 31803 Type Duplex Stainless Steel by Electrochemical Reactivation Method: A Comparative Study
title_full_unstemmed Determination of Susceptibility to Intergranular Corrosion of UNS 31803 Type Duplex Stainless Steel by Electrochemical Reactivation Method: A Comparative Study
title_sort determination of susceptibility to intergranular corrosion of uns 31803 type duplex stainless steel by electrochemical reactivation method: a comparative study
publisher Hindawi Limited
series International Journal of Corrosion
issn 1687-9325
1687-9333
publishDate 2012-01-01
description In the present study as in our previous studies (Arikan and Doruk, 2008 and Arikan et al., 2012), similar specimens taken from a hot rolled cylindrical duplex stainless steel (DSS) bar with 22% Cr grade were solution annealed at 1050°C and then aged at 800∘C from 100 to 31622 min for sensitization treatment. Double loop electrochemical potentiodynamic reactivation and standard weight loss immersion acid tests were conducted. The solution annealed samples were found unsensitized. The samples aged for 100 min were less sensitized whereas samples aged for 316 min and more time were sensitized. The degree of sensitization (DOS) can be attributed to higher contribution of chromium and molybdenum depleted areas that result from intermetallic phases. However, especially the samples aged from 3162 to 31622 min have revealed chromium replenishment. Consequently, the degree of sensitization was lowered in comparison to the results obtained in previous studies.
url http://dx.doi.org/10.1155/2012/478508
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