Quasi-Static Tensile Properties of Unalloyed Copper Produced by Electron Beam Powder Bed Fusion Additive Manufacturing

Mechanical properties of powder bed fusion processed unalloyed copper are reported majorly in the as-fabricated condition, and the effect of post-processes, common to additive manufacturing, is not well documented. In this study, mechanical properties of unalloyed copper processed by electron beam p...

Full description

Bibliographic Details
Main Authors: Prithwish Tarafder, Christopher Rock, Timothy Horn
Format: Article
Language:English
Published: MDPI AG 2021-05-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/14/11/2932
id doaj-f534ffd5c5a0486591a89f9c834a081d
record_format Article
spelling doaj-f534ffd5c5a0486591a89f9c834a081d2021-06-01T01:34:41ZengMDPI AGMaterials1996-19442021-05-01142932293210.3390/ma14112932Quasi-Static Tensile Properties of Unalloyed Copper Produced by Electron Beam Powder Bed Fusion Additive ManufacturingPrithwish Tarafder0Christopher Rock1Timothy Horn2Center for Additive Manufacturing and Logistics, Fitts-Woolard Hall, North Carolina State University, Raleigh, NC 27606, USACenter for Additive Manufacturing and Logistics, Fitts-Woolard Hall, North Carolina State University, Raleigh, NC 27606, USACenter for Additive Manufacturing and Logistics, Fitts-Woolard Hall, North Carolina State University, Raleigh, NC 27606, USAMechanical properties of powder bed fusion processed unalloyed copper are reported majorly in the as-fabricated condition, and the effect of post-processes, common to additive manufacturing, is not well documented. In this study, mechanical properties of unalloyed copper processed by electron beam powder bed fusion are characterized via room temperature quasi-static uniaxial tensile test and Vickers microhardness. Tensile samples were extracted both perpendicular and parallel to the build direction and assigned to three different conditions: as-fabricated, hot isostatic pressing (HIP), and vacuum annealing. In the as-fabricated condition, the highest UTS and lowest elongation were obtained in the samples oriented perpendicular to the build direction. These were observed to have clear trends between sample orientation caused primarily by the interdependencies between the epitaxial columnar grain morphology and dislocation movement during the tensile test. Texture was insignificant in the as-fabricated condition, and its effect on the mechanical properties was outweighed by the orientation anisotropy. The fractographs revealed a ductile mode of failure with varying dimple sizes where more shallow and finely spaced dimples were observed in the samples oriented perpendicular to the build direction. EDS maps reveal that grain boundary oxides coalesce and grow in HIP and vacuum-annealed specimens which are seen inside the ductile dimples and contribute to their increased ductility. Overall, for the post-process parameters chosen in this study, HIP was observed to slightly increase the sample’s density while vacuum annealing reduced the oxygen content in the specimens.https://www.mdpi.com/1996-1944/14/11/2932electron beampowder bed fusioncopperpost-processmechanical propertymicrostructure
collection DOAJ
language English
format Article
sources DOAJ
author Prithwish Tarafder
Christopher Rock
Timothy Horn
spellingShingle Prithwish Tarafder
Christopher Rock
Timothy Horn
Quasi-Static Tensile Properties of Unalloyed Copper Produced by Electron Beam Powder Bed Fusion Additive Manufacturing
Materials
electron beam
powder bed fusion
copper
post-process
mechanical property
microstructure
author_facet Prithwish Tarafder
Christopher Rock
Timothy Horn
author_sort Prithwish Tarafder
title Quasi-Static Tensile Properties of Unalloyed Copper Produced by Electron Beam Powder Bed Fusion Additive Manufacturing
title_short Quasi-Static Tensile Properties of Unalloyed Copper Produced by Electron Beam Powder Bed Fusion Additive Manufacturing
title_full Quasi-Static Tensile Properties of Unalloyed Copper Produced by Electron Beam Powder Bed Fusion Additive Manufacturing
title_fullStr Quasi-Static Tensile Properties of Unalloyed Copper Produced by Electron Beam Powder Bed Fusion Additive Manufacturing
title_full_unstemmed Quasi-Static Tensile Properties of Unalloyed Copper Produced by Electron Beam Powder Bed Fusion Additive Manufacturing
title_sort quasi-static tensile properties of unalloyed copper produced by electron beam powder bed fusion additive manufacturing
publisher MDPI AG
series Materials
issn 1996-1944
publishDate 2021-05-01
description Mechanical properties of powder bed fusion processed unalloyed copper are reported majorly in the as-fabricated condition, and the effect of post-processes, common to additive manufacturing, is not well documented. In this study, mechanical properties of unalloyed copper processed by electron beam powder bed fusion are characterized via room temperature quasi-static uniaxial tensile test and Vickers microhardness. Tensile samples were extracted both perpendicular and parallel to the build direction and assigned to three different conditions: as-fabricated, hot isostatic pressing (HIP), and vacuum annealing. In the as-fabricated condition, the highest UTS and lowest elongation were obtained in the samples oriented perpendicular to the build direction. These were observed to have clear trends between sample orientation caused primarily by the interdependencies between the epitaxial columnar grain morphology and dislocation movement during the tensile test. Texture was insignificant in the as-fabricated condition, and its effect on the mechanical properties was outweighed by the orientation anisotropy. The fractographs revealed a ductile mode of failure with varying dimple sizes where more shallow and finely spaced dimples were observed in the samples oriented perpendicular to the build direction. EDS maps reveal that grain boundary oxides coalesce and grow in HIP and vacuum-annealed specimens which are seen inside the ductile dimples and contribute to their increased ductility. Overall, for the post-process parameters chosen in this study, HIP was observed to slightly increase the sample’s density while vacuum annealing reduced the oxygen content in the specimens.
topic electron beam
powder bed fusion
copper
post-process
mechanical property
microstructure
url https://www.mdpi.com/1996-1944/14/11/2932
work_keys_str_mv AT prithwishtarafder quasistatictensilepropertiesofunalloyedcopperproducedbyelectronbeampowderbedfusionadditivemanufacturing
AT christopherrock quasistatictensilepropertiesofunalloyedcopperproducedbyelectronbeampowderbedfusionadditivemanufacturing
AT timothyhorn quasistatictensilepropertiesofunalloyedcopperproducedbyelectronbeampowderbedfusionadditivemanufacturing
_version_ 1721412071537508352