High Temperature Deformation of Twin-Roll Cast Al-Mn-Based Alloys after Equal Channel Angular Pressing

Twin roll cast Al-Mn- and Al-Mn-Zr-based alloys were subjected to four passes of equal channel angular pressing. The resulting grain size of 400 nm contributes to a significant strengthening at room temperature. This microstructure is not fully stable at elevated temperatures and recrystallization a...

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Main Authors: Přemysl Málek, Michaela Šlapáková Poková, Miroslav Cieslar
Format: Article
Language:English
Published: MDPI AG 2015-11-01
Series:Materials
Subjects:
TRC
Online Access:http://www.mdpi.com/1996-1944/8/11/5401
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spelling doaj-f47bb440a24c4879a54353196478df452020-11-24T21:46:33ZengMDPI AGMaterials1996-19442015-11-018117650766210.3390/ma8115401ma8115401High Temperature Deformation of Twin-Roll Cast Al-Mn-Based Alloys after Equal Channel Angular PressingPřemysl Málek0Michaela Šlapáková Poková1Miroslav Cieslar2Department of Physics of Materials, Charles University in Prague, Faculty of Mathematics and Physics, Ke Karlovu 5, Prague 2 12116, Czech RepublicDepartment of Physics of Materials, Charles University in Prague, Faculty of Mathematics and Physics, Ke Karlovu 5, Prague 2 12116, Czech RepublicDepartment of Physics of Materials, Charles University in Prague, Faculty of Mathematics and Physics, Ke Karlovu 5, Prague 2 12116, Czech RepublicTwin roll cast Al-Mn- and Al-Mn-Zr-based alloys were subjected to four passes of equal channel angular pressing. The resulting grain size of 400 nm contributes to a significant strengthening at room temperature. This microstructure is not fully stable at elevated temperatures and recrystallization and vast grain growth occur at temperatures between 350 and 450 °C. The onset of these microstructure changes depends on chemical and phase composition. Better stability is observed in the Al-Mn-Zr-based alloy. High temperature tensile tests reveal that equal channel angular pressing results in a softening of all studied materials at high temperatures. This can be explained by an active role of grain boundaries in the deformation process. The maximum values of ductility and strain rate sensitivity parameter m found in the Al-Mn-Zr-based alloy are below the bottom limit of superplasticity (155%, m = 0.25). However, some features typical for superplastic behavior were observed—the strain rate dependence of the parameter m, the strengthening with increasing grain size, and the fracture by diffuse necking. Grain boundary sliding is believed to contribute partially to the overall strain in specimens where the grain size remained in the microcrystalline range.http://www.mdpi.com/1996-1944/8/11/5401Al-Mn-based alloysTRCECAPmicrostructure stabilityhigh temperature mechanical properties
collection DOAJ
language English
format Article
sources DOAJ
author Přemysl Málek
Michaela Šlapáková Poková
Miroslav Cieslar
spellingShingle Přemysl Málek
Michaela Šlapáková Poková
Miroslav Cieslar
High Temperature Deformation of Twin-Roll Cast Al-Mn-Based Alloys after Equal Channel Angular Pressing
Materials
Al-Mn-based alloys
TRC
ECAP
microstructure stability
high temperature mechanical properties
author_facet Přemysl Málek
Michaela Šlapáková Poková
Miroslav Cieslar
author_sort Přemysl Málek
title High Temperature Deformation of Twin-Roll Cast Al-Mn-Based Alloys after Equal Channel Angular Pressing
title_short High Temperature Deformation of Twin-Roll Cast Al-Mn-Based Alloys after Equal Channel Angular Pressing
title_full High Temperature Deformation of Twin-Roll Cast Al-Mn-Based Alloys after Equal Channel Angular Pressing
title_fullStr High Temperature Deformation of Twin-Roll Cast Al-Mn-Based Alloys after Equal Channel Angular Pressing
title_full_unstemmed High Temperature Deformation of Twin-Roll Cast Al-Mn-Based Alloys after Equal Channel Angular Pressing
title_sort high temperature deformation of twin-roll cast al-mn-based alloys after equal channel angular pressing
publisher MDPI AG
series Materials
issn 1996-1944
publishDate 2015-11-01
description Twin roll cast Al-Mn- and Al-Mn-Zr-based alloys were subjected to four passes of equal channel angular pressing. The resulting grain size of 400 nm contributes to a significant strengthening at room temperature. This microstructure is not fully stable at elevated temperatures and recrystallization and vast grain growth occur at temperatures between 350 and 450 °C. The onset of these microstructure changes depends on chemical and phase composition. Better stability is observed in the Al-Mn-Zr-based alloy. High temperature tensile tests reveal that equal channel angular pressing results in a softening of all studied materials at high temperatures. This can be explained by an active role of grain boundaries in the deformation process. The maximum values of ductility and strain rate sensitivity parameter m found in the Al-Mn-Zr-based alloy are below the bottom limit of superplasticity (155%, m = 0.25). However, some features typical for superplastic behavior were observed—the strain rate dependence of the parameter m, the strengthening with increasing grain size, and the fracture by diffuse necking. Grain boundary sliding is believed to contribute partially to the overall strain in specimens where the grain size remained in the microcrystalline range.
topic Al-Mn-based alloys
TRC
ECAP
microstructure stability
high temperature mechanical properties
url http://www.mdpi.com/1996-1944/8/11/5401
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