2-{[2-(2-Hydroxy-3-methoxybenzylidene)hydrazin-1-ylidene]methyl}-6-methoxyphenol

2-{[2-(2-Hydroxy-3-methoxybenzylidene)hydrazin-1-ylidene]methyl}-6-methoxyphenol

The title compound, C16H16N2O4, was obtained from the reaction of hydrazine hydrate and o-vanilin in absolute ethanol. The molecule is almost planar (except for the methyl H atoms), with a mean deviation from the plane of 0.0259 Å. The molecular structure also exhibits an...

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Main Authors: Shunsheng Zhao, Xingqiang Lü, Wenxia Wang, Rong Lu
Format: Article
Language:English
Published: International Union of Crystallography 2011-10-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536811036816
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spelling doaj-f328e3639dbd49368e4bea27b866b1882020-11-25T01:35:45ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682011-10-016710o2702o270210.1107/S16005368110368162-{[2-(2-Hydroxy-3-methoxybenzylidene)hydrazin-1-ylidene]methyl}-6-methoxyphenolShunsheng ZhaoXingqiang LüWenxia WangRong LuThe title compound, C16H16N2O4, was obtained from the reaction of hydrazine hydrate and o-vanilin in absolute ethanol. The molecule is almost planar (except for the methyl H atoms), with a mean deviation from the plane of 0.0259 Å. The molecular structure also exhibits an approximate non-crystallographic twofold axis. Intramolecular O—H...N hydrogen bonds occur. In the crystal, intermolecular C—H...O hydrogen bonds generate molecular zigzag sheets. The sheets stack through C—H...π interactions, leading to a three-dimensional-network.http://scripts.iucr.org/cgi-bin/paper?S1600536811036816
collection DOAJ
language English
format Article
sources DOAJ
author Shunsheng Zhao
Xingqiang Lü
Wenxia Wang
Rong Lu
spellingShingle Shunsheng Zhao
Xingqiang Lü
Wenxia Wang
Rong Lu
2-{[2-(2-Hydroxy-3-methoxybenzylidene)hydrazin-1-ylidene]methyl}-6-methoxyphenol
Acta Crystallographica Section E
author_facet Shunsheng Zhao
Xingqiang Lü
Wenxia Wang
Rong Lu
author_sort Shunsheng Zhao
title 2-{[2-(2-Hydroxy-3-methoxybenzylidene)hydrazin-1-ylidene]methyl}-6-methoxyphenol
title_short 2-{[2-(2-Hydroxy-3-methoxybenzylidene)hydrazin-1-ylidene]methyl}-6-methoxyphenol
title_full 2-{[2-(2-Hydroxy-3-methoxybenzylidene)hydrazin-1-ylidene]methyl}-6-methoxyphenol
title_fullStr 2-{[2-(2-Hydroxy-3-methoxybenzylidene)hydrazin-1-ylidene]methyl}-6-methoxyphenol
title_full_unstemmed 2-{[2-(2-Hydroxy-3-methoxybenzylidene)hydrazin-1-ylidene]methyl}-6-methoxyphenol
title_sort 2-{[2-(2-hydroxy-3-methoxybenzylidene)hydrazin-1-ylidene]methyl}-6-methoxyphenol
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2011-10-01
description The title compound, C16H16N2O4, was obtained from the reaction of hydrazine hydrate and o-vanilin in absolute ethanol. The molecule is almost planar (except for the methyl H atoms), with a mean deviation from the plane of 0.0259 Å. The molecular structure also exhibits an approximate non-crystallographic twofold axis. Intramolecular O—H...N hydrogen bonds occur. In the crystal, intermolecular C—H...O hydrogen bonds generate molecular zigzag sheets. The sheets stack through C—H...π interactions, leading to a three-dimensional-network.
url http://scripts.iucr.org/cgi-bin/paper?S1600536811036816
work_keys_str_mv AT shunshengzhao 222hydroxy3methoxybenzylidenehydrazin1ylidenemethyl6methoxyphenol
AT xingqianglamp252 222hydroxy3methoxybenzylidenehydrazin1ylidenemethyl6methoxyphenol
AT wenxiawang 222hydroxy3methoxybenzylidenehydrazin1ylidenemethyl6methoxyphenol
AT ronglu 222hydroxy3methoxybenzylidenehydrazin1ylidenemethyl6methoxyphenol
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