Experimental investigation into the effects of composition and microstructure on the tensile properties and failure characteristics of different gypsum rocks

Abstract The present work investigated the differences in the composition and internal microstructure of four types gypsum rock—fiber gypsum, transparent gypsum, alabaster, and ordinary gypsum by X-ray fluorescence spectrometry, X-ray diffraction, scanning electron microscope and Brazilian split tes...

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Main Authors: Hongfa Ma, Shaojie Chen, Yanqi Song, Dawei Yin, Xiangshang Li, Xiaolong Li
Format: Article
Language:English
Published: Nature Publishing Group 2021-07-01
Series:Scientific Reports
Online Access:https://doi.org/10.1038/s41598-021-93947-6
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spelling doaj-f1ffb17683b14266946e4b0881c21ce42021-07-18T11:28:22ZengNature Publishing GroupScientific Reports2045-23222021-07-0111111310.1038/s41598-021-93947-6Experimental investigation into the effects of composition and microstructure on the tensile properties and failure characteristics of different gypsum rocksHongfa Ma0Shaojie Chen1Yanqi Song2Dawei Yin3Xiangshang Li4Xiaolong Li5School of Mechanics and Civil Engineering, China University of Mining and Technology (Beijing)State Key Laboratory of Mine Disaster Prevention and Control, Shandong University of Science and TechnologyState Key Laboratory for GeoMechanics and Deep Underground Engineering, China University of Mining and Technology (Beijing)State Key Laboratory of Mine Disaster Prevention and Control, Shandong University of Science and TechnologySchool of Mechanics and Civil Engineering, China University of Mining and Technology (Beijing)School of Mechanics and Civil Engineering, China University of Mining and Technology (Beijing)Abstract The present work investigated the differences in the composition and internal microstructure of four types gypsum rock—fiber gypsum, transparent gypsum, alabaster, and ordinary gypsum by X-ray fluorescence spectrometry, X-ray diffraction, scanning electron microscope and Brazilian split test, and analyzed its effects on the tensile strength and fracture characteristics of gypsum rock. For alabaster, fiber gypsum, transparent gypsum, and ordinary gypsum, CaSO4·2H2O is the main component with 72.78%, 72.72%, 72.57%, and 71.51% content, and tensile strength of 1.79, 2.22, 3.22, and 4.35 MPa, respectively. In addition, the fracture line is arc-shaped, vertical, and zigzag for fiber gypsum, ordinary and transparent gypsums, and alabaster, respectively. On the microscopic level, fiber gypsum has an evident striated structure while the gradual increased pore development for alabaster, transparent gypsum, and ordinary gypsum. Gypsum rock has an obvious layered crystal structure with the increase of CaSO4·2H2O, contributing to the phenomenon with a larger grain size and lower tensile strength. In addition, the number of particles for alabaster, transparent gypsum, and ordinary gypsum increased in turn, while their particle size decreased uniformly, indicating that the lower CaSO4·2H2O content, the more sufficient energy accumulation and release. This paper can provide a theoretical basis for the analysis of the mechanical properties of rocks with different mineral composition and contribute to the design for different ore grades mining.https://doi.org/10.1038/s41598-021-93947-6
collection DOAJ
language English
format Article
sources DOAJ
author Hongfa Ma
Shaojie Chen
Yanqi Song
Dawei Yin
Xiangshang Li
Xiaolong Li
spellingShingle Hongfa Ma
Shaojie Chen
Yanqi Song
Dawei Yin
Xiangshang Li
Xiaolong Li
Experimental investigation into the effects of composition and microstructure on the tensile properties and failure characteristics of different gypsum rocks
Scientific Reports
author_facet Hongfa Ma
Shaojie Chen
Yanqi Song
Dawei Yin
Xiangshang Li
Xiaolong Li
author_sort Hongfa Ma
title Experimental investigation into the effects of composition and microstructure on the tensile properties and failure characteristics of different gypsum rocks
title_short Experimental investigation into the effects of composition and microstructure on the tensile properties and failure characteristics of different gypsum rocks
title_full Experimental investigation into the effects of composition and microstructure on the tensile properties and failure characteristics of different gypsum rocks
title_fullStr Experimental investigation into the effects of composition and microstructure on the tensile properties and failure characteristics of different gypsum rocks
title_full_unstemmed Experimental investigation into the effects of composition and microstructure on the tensile properties and failure characteristics of different gypsum rocks
title_sort experimental investigation into the effects of composition and microstructure on the tensile properties and failure characteristics of different gypsum rocks
publisher Nature Publishing Group
series Scientific Reports
issn 2045-2322
publishDate 2021-07-01
description Abstract The present work investigated the differences in the composition and internal microstructure of four types gypsum rock—fiber gypsum, transparent gypsum, alabaster, and ordinary gypsum by X-ray fluorescence spectrometry, X-ray diffraction, scanning electron microscope and Brazilian split test, and analyzed its effects on the tensile strength and fracture characteristics of gypsum rock. For alabaster, fiber gypsum, transparent gypsum, and ordinary gypsum, CaSO4·2H2O is the main component with 72.78%, 72.72%, 72.57%, and 71.51% content, and tensile strength of 1.79, 2.22, 3.22, and 4.35 MPa, respectively. In addition, the fracture line is arc-shaped, vertical, and zigzag for fiber gypsum, ordinary and transparent gypsums, and alabaster, respectively. On the microscopic level, fiber gypsum has an evident striated structure while the gradual increased pore development for alabaster, transparent gypsum, and ordinary gypsum. Gypsum rock has an obvious layered crystal structure with the increase of CaSO4·2H2O, contributing to the phenomenon with a larger grain size and lower tensile strength. In addition, the number of particles for alabaster, transparent gypsum, and ordinary gypsum increased in turn, while their particle size decreased uniformly, indicating that the lower CaSO4·2H2O content, the more sufficient energy accumulation and release. This paper can provide a theoretical basis for the analysis of the mechanical properties of rocks with different mineral composition and contribute to the design for different ore grades mining.
url https://doi.org/10.1038/s41598-021-93947-6
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