2-(3,4-Dimethoxyphenyl)-<i>N</i>-(4-methoxyphenyl)-1-propyl-1<i>H</i>-benzo[<i>d</i>]imidazole-5-carboxamide

2-(3,4-Dimethoxyphenyl)-<i>N</i>-(4-methoxyphenyl)-1-propyl-1<i>H</i>-benzo[<i>d</i>]imidazole-5-carboxamide

2-(3,4-Dimethoxyphenyl)-<i>N</i>-(4-methoxyphenyl)-1-propyl-1<i>H</i>-benzo[<i>d</i>]imidazole-5-carboxamide was synthesized by the &#8216;one-pot&#8217; reductive cyclization of <i>N</i>-(4-methoxyphenyl)-3-nitro-4-(propylamino)benzamide with...

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Main Authors: Prakash Bhaskar, Vasantha Kumar, Suresha Kumara Tholappanavara Hanumanthappa, Sowmya Haliwana Banakara Vijaykumar
Format: Article
Language:English
Published: MDPI AG 2019-09-01
Series:Molbank
Subjects:
benzimidazole
carboxamide
one-pot synthesis
reductive cyclization
Online Access:https://www.mdpi.com/1422-8599/2019/3/M1079
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spelling doaj-eb6de30929ed4e82a7c033c4e3e51dcd2020-11-24T20:53:05ZengMDPI AGMolbank1422-85992019-09-0120193M107910.3390/M1079M10792-(3,4-Dimethoxyphenyl)-<i>N</i>-(4-methoxyphenyl)-1-propyl-1<i>H</i>-benzo[<i>d</i>]imidazole-5-carboxamidePrakash Bhaskar0Vasantha Kumar1Suresha Kumara Tholappanavara Hanumanthappa2Sowmya Haliwana Banakara Vijaykumar3Department of Chemistry, Centre for Research in Social Sciences and Education, Jain University 52, Bellary Road, Hebbal, Bangalore-560024, Karnataka, IndiaSri Dharmashthala Manjunatheshwara College (Autonomous), Ujire-574240, Karnataka, IndiaDepartment of Chemistry, U.B.D.T. College of Engineering (A Constituent College of Visvesvaraya Technological University), Davanagere-577004, Karnataka, IndiaDepartment of Chemistry, Centre for Research in Social Sciences and Education, Jain University 52, Bellary Road, Hebbal, Bangalore-560024, Karnataka, India2-(3,4-Dimethoxyphenyl)-<i>N</i>-(4-methoxyphenyl)-1-propyl-1<i>H</i>-benzo[<i>d</i>]imidazole-5-carboxamide was synthesized by the &#8216;one-pot&#8217; reductive cyclization of <i>N</i>-(4-methoxyphenyl)-3-nitro-4-(propylamino)benzamide with 3,4-dimethoxybenzaldehyde, using sodium dithionite as a reductive cyclizing agent using DMSO as a solvent. The structure of newly synthesized compound was elucidated based on IR, <sup>1</sup>H-NMR, <sup>13</sup>C-NMR, and LC-MS data.https://www.mdpi.com/1422-8599/2019/3/M1079benzimidazolecarboxamideone-pot synthesisreductive cyclization
collection DOAJ
language English
format Article
sources DOAJ
author Prakash Bhaskar
Vasantha Kumar
Suresha Kumara Tholappanavara Hanumanthappa
Sowmya Haliwana Banakara Vijaykumar
spellingShingle Prakash Bhaskar
Vasantha Kumar
Suresha Kumara Tholappanavara Hanumanthappa
Sowmya Haliwana Banakara Vijaykumar
2-(3,4-Dimethoxyphenyl)-<i>N</i>-(4-methoxyphenyl)-1-propyl-1<i>H</i>-benzo[<i>d</i>]imidazole-5-carboxamide
Molbank
benzimidazole
carboxamide
one-pot synthesis
reductive cyclization
author_facet Prakash Bhaskar
Vasantha Kumar
Suresha Kumara Tholappanavara Hanumanthappa
Sowmya Haliwana Banakara Vijaykumar
author_sort Prakash Bhaskar
title 2-(3,4-Dimethoxyphenyl)-<i>N</i>-(4-methoxyphenyl)-1-propyl-1<i>H</i>-benzo[<i>d</i>]imidazole-5-carboxamide
title_short 2-(3,4-Dimethoxyphenyl)-<i>N</i>-(4-methoxyphenyl)-1-propyl-1<i>H</i>-benzo[<i>d</i>]imidazole-5-carboxamide
title_full 2-(3,4-Dimethoxyphenyl)-<i>N</i>-(4-methoxyphenyl)-1-propyl-1<i>H</i>-benzo[<i>d</i>]imidazole-5-carboxamide
title_fullStr 2-(3,4-Dimethoxyphenyl)-<i>N</i>-(4-methoxyphenyl)-1-propyl-1<i>H</i>-benzo[<i>d</i>]imidazole-5-carboxamide
title_full_unstemmed 2-(3,4-Dimethoxyphenyl)-<i>N</i>-(4-methoxyphenyl)-1-propyl-1<i>H</i>-benzo[<i>d</i>]imidazole-5-carboxamide
title_sort 2-(3,4-dimethoxyphenyl)-<i>n</i>-(4-methoxyphenyl)-1-propyl-1<i>h</i>-benzo[<i>d</i>]imidazole-5-carboxamide
publisher MDPI AG
series Molbank
issn 1422-8599
publishDate 2019-09-01
description 2-(3,4-Dimethoxyphenyl)-<i>N</i>-(4-methoxyphenyl)-1-propyl-1<i>H</i>-benzo[<i>d</i>]imidazole-5-carboxamide was synthesized by the &#8216;one-pot&#8217; reductive cyclization of <i>N</i>-(4-methoxyphenyl)-3-nitro-4-(propylamino)benzamide with 3,4-dimethoxybenzaldehyde, using sodium dithionite as a reductive cyclizing agent using DMSO as a solvent. The structure of newly synthesized compound was elucidated based on IR, <sup>1</sup>H-NMR, <sup>13</sup>C-NMR, and LC-MS data.
topic benzimidazole
carboxamide
one-pot synthesis
reductive cyclization
url https://www.mdpi.com/1422-8599/2019/3/M1079
work_keys_str_mv AT prakashbhaskar 234dimethoxyphenylini4methoxyphenyl1propyl1ihibenzoidiimidazole5carboxamide
AT vasanthakumar 234dimethoxyphenylini4methoxyphenyl1propyl1ihibenzoidiimidazole5carboxamide
AT sureshakumaratholappanavarahanumanthappa 234dimethoxyphenylini4methoxyphenyl1propyl1ihibenzoidiimidazole5carboxamide
AT sowmyahaliwanabanakaravijaykumar 234dimethoxyphenylini4methoxyphenyl1propyl1ihibenzoidiimidazole5carboxamide
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