2,2-Bis[3,5-bis(dimethylamino)phenyl]-1,1,1,3,3,3-hexamethyltrisilane

The title compound, C26H48N4Si3, was synthesized by the reaction of 2,2-dichlorotrisilane with 3,5-bis(dimethylamino)phenyllithium. In the molecule, the dihedral angle between the benzene rings is 57.57 (7)° and the Si—Si—Si bond angle is 110.08 (2)°. In the crystal, molecules are linked via an SiC–...

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Main Authors:	Yoshiyuki Mizuhata, Kento Iwai, Norihiro Tokitoh
Format:	Article
Language:	English
Published:	International Union of Crystallography 2020-09-01
Series:	IUCrData
Subjects:	crystal structure trisilane 3,5-bis(dimethylamino)phenyl
Online Access:	http://scripts.iucr.org/cgi-bin/paper?S2414314620012997

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spelling	doaj-e9d15dd63d48425086c217939ce2e7842020-11-25T03:47:52ZengInternational Union of CrystallographyIUCrData2414-31462020-09-0159x20129910.1107/S2414314620012997is40442,2-Bis[3,5-bis(dimethylamino)phenyl]-1,1,1,3,3,3-hexamethyltrisilaneYoshiyuki Mizuhata0Kento Iwai1Norihiro Tokitoh2Institute for Chemical Research, Kyoto University, Gokasho, Uji, Kyoto 611-0011, JapanInstitute for Chemical Research, Kyoto University, Gokasho, Uji, Kyoto 611-0011, JapanInstitute for Chemical Research, Kyoto University, Gokasho, Uji, Kyoto 611-0011, JapanThe title compound, C26H48N4Si3, was synthesized by the reaction of 2,2-dichlorotrisilane with 3,5-bis(dimethylamino)phenyllithium. In the molecule, the dihedral angle between the benzene rings is 57.57 (7)° and the Si—Si—Si bond angle is 110.08 (2)°. In the crystal, molecules are linked via an SiC–H...π(aryl) interaction, forming a chain along the c-axis direction.http://scripts.iucr.org/cgi-bin/paper?S2414314620012997crystal structuretrisilane3,5-bis(dimethylamino)phenyl
collection	DOAJ
language	English
format	Article
sources	DOAJ
author	Yoshiyuki Mizuhata Kento Iwai Norihiro Tokitoh
spellingShingle	Yoshiyuki Mizuhata Kento Iwai Norihiro Tokitoh 2,2-Bis[3,5-bis(dimethylamino)phenyl]-1,1,1,3,3,3-hexamethyltrisilane IUCrData crystal structure trisilane 3,5-bis(dimethylamino)phenyl
author_facet	Yoshiyuki Mizuhata Kento Iwai Norihiro Tokitoh
author_sort	Yoshiyuki Mizuhata
title	2,2-Bis[3,5-bis(dimethylamino)phenyl]-1,1,1,3,3,3-hexamethyltrisilane
title_short	2,2-Bis[3,5-bis(dimethylamino)phenyl]-1,1,1,3,3,3-hexamethyltrisilane
title_full	2,2-Bis[3,5-bis(dimethylamino)phenyl]-1,1,1,3,3,3-hexamethyltrisilane
title_fullStr	2,2-Bis[3,5-bis(dimethylamino)phenyl]-1,1,1,3,3,3-hexamethyltrisilane
title_full_unstemmed	2,2-Bis[3,5-bis(dimethylamino)phenyl]-1,1,1,3,3,3-hexamethyltrisilane
title_sort	2,2-bis[3,5-bis(dimethylamino)phenyl]-1,1,1,3,3,3-hexamethyltrisilane
publisher	International Union of Crystallography
series	IUCrData
issn	2414-3146
publishDate	2020-09-01
description	The title compound, C26H48N4Si3, was synthesized by the reaction of 2,2-dichlorotrisilane with 3,5-bis(dimethylamino)phenyllithium. In the molecule, the dihedral angle between the benzene rings is 57.57 (7)° and the Si—Si—Si bond angle is 110.08 (2)°. In the crystal, molecules are linked via an SiC–H...π(aryl) interaction, forming a chain along the c-axis direction.
topic	crystal structure trisilane 3,5-bis(dimethylamino)phenyl
url	http://scripts.iucr.org/cgi-bin/paper?S2414314620012997
work_keys_str_mv	AT yoshiyukimizuhata 22bis35bisdimethylaminophenyl111333hexamethyltrisilane AT kentoiwai 22bis35bisdimethylaminophenyl111333hexamethyltrisilane AT norihirotokitoh 22bis35bisdimethylaminophenyl111333hexamethyltrisilane
_version_	1724501527399235584

2,2-Bis[3,5-bis(dimethylamino)phenyl]-1,1,1,3,3,3-hexamethyltrisilane

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