One Pot Synthesis of Polyhydroquinolines Catalyzed by Sulfonic Acid Functionalized SBA-15 as a New Nanoporous Acid Catalyst under Solvent Free Conditions
Sulfonic acid functionalized SBA-15 (SBA-Pr-SO3H) as a new nanoporous acid catalyst was used in the one-pot synthesis of polyhydroquinolines derivatives via the Hantzsch four component condensation reaction of aldehydes, b-ketoesters, dimedone and ammonium acetate under solvent free conditions with...
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Iranian Institute of Research and Development in Chemical Industries (IRDCI)-ACECR
2010-06-01
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| Series: | Iranian Journal of Chemistry & Chemical Engineering |
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| Online Access: | http://www.ijcce.ac.ir/article_6687_a7e84ebe49c5618e54af1f2fe294fe00.pdf |
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doaj-e76744ac34704fdeb85370d174f231fe2020-11-25T03:38:21ZengIranian Institute of Research and Development in Chemical Industries (IRDCI)-ACECRIranian Journal of Chemistry & Chemical Engineering 1021-99861021-99862010-06-012921106687One Pot Synthesis of Polyhydroquinolines Catalyzed by Sulfonic Acid Functionalized SBA-15 as a New Nanoporous Acid Catalyst under Solvent Free ConditionsGhodsi Mohammadi Ziarani0Ali Reza Badiei1Yeganeh Khaniania2Mahbobeh Haddadpour3Department of Chemistry, University of Alzahra, Tehran, I.R. IRANFaculty of Chemistry, University of Tehran, Tehran, I.R. IRANFaculty of Chemistry, University of Tehran, Tehran, I.R. IRANDepartment of Chemistry, University of Alzahra, Tehran, I.R. IRANSulfonic acid functionalized SBA-15 (SBA-Pr-SO3H) as a new nanoporous acid catalyst was used in the one-pot synthesis of polyhydroquinolines derivatives via the Hantzsch four component condensation reaction of aldehydes, b-ketoesters, dimedone and ammonium acetate under solvent free conditions with short reaction time in excellent yields. SBA-Pr-SO3H was proved to be an efficient heterogeneous nanoporous solid acid catalyst (pore size 6 nm), which could be easily handled and removed from the reaction mixture by simple filtration, and also recovered and reused without loss of reactivity.http://www.ijcce.ac.ir/article_6687_a7e84ebe49c5618e54af1f2fe294fe00.pdfnanoporous solid acid catalystsulfonic acid functionalized sba-15polyhydroquinolinessolvent free conditionsdimedone |
| collection |
DOAJ |
| language |
English |
| format |
Article |
| sources |
DOAJ |
| author |
Ghodsi Mohammadi Ziarani Ali Reza Badiei Yeganeh Khaniania Mahbobeh Haddadpour |
| spellingShingle |
Ghodsi Mohammadi Ziarani Ali Reza Badiei Yeganeh Khaniania Mahbobeh Haddadpour One Pot Synthesis of Polyhydroquinolines Catalyzed by Sulfonic Acid Functionalized SBA-15 as a New Nanoporous Acid Catalyst under Solvent Free Conditions Iranian Journal of Chemistry & Chemical Engineering nanoporous solid acid catalyst sulfonic acid functionalized sba-15 polyhydroquinolines solvent free conditions dimedone |
| author_facet |
Ghodsi Mohammadi Ziarani Ali Reza Badiei Yeganeh Khaniania Mahbobeh Haddadpour |
| author_sort |
Ghodsi Mohammadi Ziarani |
| title |
One Pot Synthesis of Polyhydroquinolines Catalyzed by Sulfonic Acid Functionalized SBA-15 as a New Nanoporous Acid Catalyst under Solvent Free Conditions |
| title_short |
One Pot Synthesis of Polyhydroquinolines Catalyzed by Sulfonic Acid Functionalized SBA-15 as a New Nanoporous Acid Catalyst under Solvent Free Conditions |
| title_full |
One Pot Synthesis of Polyhydroquinolines Catalyzed by Sulfonic Acid Functionalized SBA-15 as a New Nanoporous Acid Catalyst under Solvent Free Conditions |
| title_fullStr |
One Pot Synthesis of Polyhydroquinolines Catalyzed by Sulfonic Acid Functionalized SBA-15 as a New Nanoporous Acid Catalyst under Solvent Free Conditions |
| title_full_unstemmed |
One Pot Synthesis of Polyhydroquinolines Catalyzed by Sulfonic Acid Functionalized SBA-15 as a New Nanoporous Acid Catalyst under Solvent Free Conditions |
| title_sort |
one pot synthesis of polyhydroquinolines catalyzed by sulfonic acid functionalized sba-15 as a new nanoporous acid catalyst under solvent free conditions |
| publisher |
Iranian Institute of Research and Development in Chemical Industries (IRDCI)-ACECR |
| series |
Iranian Journal of Chemistry & Chemical Engineering |
| issn |
1021-9986 1021-9986 |
| publishDate |
2010-06-01 |
| description |
Sulfonic acid functionalized SBA-15 (SBA-Pr-SO3H) as a new nanoporous acid catalyst was used in the one-pot synthesis of polyhydroquinolines derivatives via the Hantzsch four component condensation reaction of aldehydes, b-ketoesters, dimedone and ammonium acetate under solvent free conditions with short reaction time in excellent yields. SBA-Pr-SO3H was proved to be an efficient heterogeneous nanoporous solid acid catalyst (pore size 6 nm), which could be easily handled and removed from the reaction mixture by simple filtration, and also recovered and reused without loss of reactivity. |
| topic |
nanoporous solid acid catalyst sulfonic acid functionalized sba-15 polyhydroquinolines solvent free conditions dimedone |
| url |
http://www.ijcce.ac.ir/article_6687_a7e84ebe49c5618e54af1f2fe294fe00.pdf |
| work_keys_str_mv |
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