Hot Deformation and Dynamic Recrystallisation Behaviour of Twin-Roll Cast Mg-6.8Y-2.5Zn-0.4Zr Magnesium Alloy

In this work, the deformation behaviour of a twin-roll cast (TRC) Mg-6.8Y-2.5Zn-0.4Zr alloy during plane strain compression was characterised by high-temperature testing. Based on the experimental data, the values of strain-rate sensitivity, the efficiency of power dissipation and the instability pa...

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Main Authors: Madlen Ullmann, Kristina Kittner, Ulrich Prahl
Format: Article
Language:English
Published: MDPI AG 2021-01-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/14/2/307
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spelling doaj-e4b11b52c54b4ba8863f352e1ee5906e2021-01-09T00:06:24ZengMDPI AGMaterials1996-19442021-01-011430730710.3390/ma14020307Hot Deformation and Dynamic Recrystallisation Behaviour of Twin-Roll Cast Mg-6.8Y-2.5Zn-0.4Zr Magnesium AlloyMadlen Ullmann0Kristina Kittner1Ulrich Prahl2Institute of Metal Forming, Technische Universität Bergakademie Freiberg, Bernhard-von-Cotta-Straße 4, 09599 Freiberg, GermanyInstitute of Metal Forming, Technische Universität Bergakademie Freiberg, Bernhard-von-Cotta-Straße 4, 09599 Freiberg, GermanyInstitute of Metal Forming, Technische Universität Bergakademie Freiberg, Bernhard-von-Cotta-Straße 4, 09599 Freiberg, GermanyIn this work, the deformation behaviour of a twin-roll cast (TRC) Mg-6.8Y-2.5Zn-0.4Zr alloy during plane strain compression was characterised by high-temperature testing. Based on the experimental data, the values of strain-rate sensitivity, the efficiency of power dissipation and the instability parameter were investigated under the conditions of various hot deformation parameters. In contrast to conventionally cast material, no lamellae of the LPSO (long period stacking ordered) phase were precipitated in the magnesium matrix after TRC. The precipitation of fine lamellar LPSO phases only occurred during cooling to forming temperature after the heat treatment. Dynamic recrystallization (DRX) hardly occurred during deformation at temperatures between 350 °C and 400 °C. This can be attributed to the precipitation of the lamellar LSPO phases, which contribute to retardation of the DRX process. At higher deformation temperatures and strain rates DRX is pronounced and the twin-induced (TRDX) as well as continuous dynamic recrystallization could be identified as the dominant softening mechanisms. The processing maps were established by superimposing the instability map over the power dissipation map, this being associated with microstructural evolution analysis in the hot deformation processes. Two instability zones could be recognised for the twin-roll cast and heat-treated Mg-6.8Y-2.5Zn-0.4Zr alloy: (1) 350 °C to 460 °C and 0.01 s<sup>−1</sup> to 0.3 s<sup>−1</sup> and (2) 485 °C to 525 °C and 2.5 s<sup>−1</sup> to 10 s<sup>−1</sup>, where deformation is not favourable.https://www.mdpi.com/1996-1944/14/2/307flow curvedynamic recrystallisationprocessing mapLPSO phaseMg-6.8Y-2.5Zn-0.4Zrtwin-roll casting
collection DOAJ
language English
format Article
sources DOAJ
author Madlen Ullmann
Kristina Kittner
Ulrich Prahl
spellingShingle Madlen Ullmann
Kristina Kittner
Ulrich Prahl
Hot Deformation and Dynamic Recrystallisation Behaviour of Twin-Roll Cast Mg-6.8Y-2.5Zn-0.4Zr Magnesium Alloy
Materials
flow curve
dynamic recrystallisation
processing map
LPSO phase
Mg-6.8Y-2.5Zn-0.4Zr
twin-roll casting
author_facet Madlen Ullmann
Kristina Kittner
Ulrich Prahl
author_sort Madlen Ullmann
title Hot Deformation and Dynamic Recrystallisation Behaviour of Twin-Roll Cast Mg-6.8Y-2.5Zn-0.4Zr Magnesium Alloy
title_short Hot Deformation and Dynamic Recrystallisation Behaviour of Twin-Roll Cast Mg-6.8Y-2.5Zn-0.4Zr Magnesium Alloy
title_full Hot Deformation and Dynamic Recrystallisation Behaviour of Twin-Roll Cast Mg-6.8Y-2.5Zn-0.4Zr Magnesium Alloy
title_fullStr Hot Deformation and Dynamic Recrystallisation Behaviour of Twin-Roll Cast Mg-6.8Y-2.5Zn-0.4Zr Magnesium Alloy
title_full_unstemmed Hot Deformation and Dynamic Recrystallisation Behaviour of Twin-Roll Cast Mg-6.8Y-2.5Zn-0.4Zr Magnesium Alloy
title_sort hot deformation and dynamic recrystallisation behaviour of twin-roll cast mg-6.8y-2.5zn-0.4zr magnesium alloy
publisher MDPI AG
series Materials
issn 1996-1944
publishDate 2021-01-01
description In this work, the deformation behaviour of a twin-roll cast (TRC) Mg-6.8Y-2.5Zn-0.4Zr alloy during plane strain compression was characterised by high-temperature testing. Based on the experimental data, the values of strain-rate sensitivity, the efficiency of power dissipation and the instability parameter were investigated under the conditions of various hot deformation parameters. In contrast to conventionally cast material, no lamellae of the LPSO (long period stacking ordered) phase were precipitated in the magnesium matrix after TRC. The precipitation of fine lamellar LPSO phases only occurred during cooling to forming temperature after the heat treatment. Dynamic recrystallization (DRX) hardly occurred during deformation at temperatures between 350 °C and 400 °C. This can be attributed to the precipitation of the lamellar LSPO phases, which contribute to retardation of the DRX process. At higher deformation temperatures and strain rates DRX is pronounced and the twin-induced (TRDX) as well as continuous dynamic recrystallization could be identified as the dominant softening mechanisms. The processing maps were established by superimposing the instability map over the power dissipation map, this being associated with microstructural evolution analysis in the hot deformation processes. Two instability zones could be recognised for the twin-roll cast and heat-treated Mg-6.8Y-2.5Zn-0.4Zr alloy: (1) 350 °C to 460 °C and 0.01 s<sup>−1</sup> to 0.3 s<sup>−1</sup> and (2) 485 °C to 525 °C and 2.5 s<sup>−1</sup> to 10 s<sup>−1</sup>, where deformation is not favourable.
topic flow curve
dynamic recrystallisation
processing map
LPSO phase
Mg-6.8Y-2.5Zn-0.4Zr
twin-roll casting
url https://www.mdpi.com/1996-1944/14/2/307
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