Production of Reducing Sugar from Cassava Solid Waste by Simultaneous Ultrasonication and Acid Hydrolysis

In this study, acid hydrolysis of cassava solid waste under ultrasound irradiation for reducing sugar production was studied. A series of experiments was carried out under a 40 kHz ultrasound irradiation, with the main purpose to examine the effect of pHs, hydrolysis times, and temperatures on the c...

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Main Authors: Wasinton Simanjuntak, Heri Satria, Nurul Utami
Format: Article
Language:English
Published: Universitas Gadjah Mada 2014-10-01
Series:Indonesian Journal of Chemistry
Subjects:
Online Access:https://jurnal.ugm.ac.id/ijc/article/view/21233
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spelling doaj-e39d2a4640c646b7a3fe6ca2571df2e12020-11-24T22:23:03ZengUniversitas Gadjah MadaIndonesian Journal of Chemistry1411-94202460-15782014-10-0114323323810.22146/ijc.2123314331Production of Reducing Sugar from Cassava Solid Waste by Simultaneous Ultrasonication and Acid HydrolysisWasinton Simanjuntak0Heri Satria1Nurul Utami2Department of Chemistry, Faculty of Mathematics and Natural Sciences, University of Lampung, Jl. Soemantri Brojonegoro No. 1 Bandar Lampung 35145Department of Chemistry, Faculty of Mathematics and Natural Sciences, University of Lampung, Jl. Soemantri Brojonegoro No. 1 Bandar Lampung 35145Department of Chemistry, Faculty of Mathematics and Natural Sciences, University of Lampung, Jl. Soemantri Brojonegoro No. 1 Bandar Lampung 35145In this study, acid hydrolysis of cassava solid waste under ultrasound irradiation for reducing sugar production was studied. A series of experiments was carried out under a 40 kHz ultrasound irradiation, with the main purpose to examine the effect of pHs, hydrolysis times, and temperatures on the concentration of reducing sugar produced. As a control an untreated sample was subjected to thermal hydrolysis under the optimum condition obtained from the hydrolysis experiments under ultrasound treatment. The results obtained indicated that the highest reducing sugar concentration was obtained from the experiment undertaken at pH = 2.0; hydrolysis time of 90 min, and temperature of 80 °C. Experiment conducted at this optimum condition was found to produce reducing sugar with the concentration of 801 mg/L. This concentration around 11 times over that produced from control sample, demonstrating that simultaneous ultrasonication and hydrolysis is far more effective than conventional thermal hydrolysis. This hydrolysis improvement is attributed to the ultrasound stimulated degradation of starch molecules, leading to accelerated hydrolysis due to the cavitations of the molecules, as evidently shown by the result of SEM characterization of the original and ultrasonicated sample.https://jurnal.ugm.ac.id/ijc/article/view/21233cassava solid wasteultrasoundreducing sugar
collection DOAJ
language English
format Article
sources DOAJ
author Wasinton Simanjuntak
Heri Satria
Nurul Utami
spellingShingle Wasinton Simanjuntak
Heri Satria
Nurul Utami
Production of Reducing Sugar from Cassava Solid Waste by Simultaneous Ultrasonication and Acid Hydrolysis
Indonesian Journal of Chemistry
cassava solid waste
ultrasound
reducing sugar
author_facet Wasinton Simanjuntak
Heri Satria
Nurul Utami
author_sort Wasinton Simanjuntak
title Production of Reducing Sugar from Cassava Solid Waste by Simultaneous Ultrasonication and Acid Hydrolysis
title_short Production of Reducing Sugar from Cassava Solid Waste by Simultaneous Ultrasonication and Acid Hydrolysis
title_full Production of Reducing Sugar from Cassava Solid Waste by Simultaneous Ultrasonication and Acid Hydrolysis
title_fullStr Production of Reducing Sugar from Cassava Solid Waste by Simultaneous Ultrasonication and Acid Hydrolysis
title_full_unstemmed Production of Reducing Sugar from Cassava Solid Waste by Simultaneous Ultrasonication and Acid Hydrolysis
title_sort production of reducing sugar from cassava solid waste by simultaneous ultrasonication and acid hydrolysis
publisher Universitas Gadjah Mada
series Indonesian Journal of Chemistry
issn 1411-9420
2460-1578
publishDate 2014-10-01
description In this study, acid hydrolysis of cassava solid waste under ultrasound irradiation for reducing sugar production was studied. A series of experiments was carried out under a 40 kHz ultrasound irradiation, with the main purpose to examine the effect of pHs, hydrolysis times, and temperatures on the concentration of reducing sugar produced. As a control an untreated sample was subjected to thermal hydrolysis under the optimum condition obtained from the hydrolysis experiments under ultrasound treatment. The results obtained indicated that the highest reducing sugar concentration was obtained from the experiment undertaken at pH = 2.0; hydrolysis time of 90 min, and temperature of 80 °C. Experiment conducted at this optimum condition was found to produce reducing sugar with the concentration of 801 mg/L. This concentration around 11 times over that produced from control sample, demonstrating that simultaneous ultrasonication and hydrolysis is far more effective than conventional thermal hydrolysis. This hydrolysis improvement is attributed to the ultrasound stimulated degradation of starch molecules, leading to accelerated hydrolysis due to the cavitations of the molecules, as evidently shown by the result of SEM characterization of the original and ultrasonicated sample.
topic cassava solid waste
ultrasound
reducing sugar
url https://jurnal.ugm.ac.id/ijc/article/view/21233
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AT herisatria productionofreducingsugarfromcassavasolidwastebysimultaneousultrasonicationandacidhydrolysis
AT nurulutami productionofreducingsugarfromcassavasolidwastebysimultaneousultrasonicationandacidhydrolysis
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