Plastic deformation of synthetic quartz nanopillars by nanoindentation for multi-scale and multi-level security artefact metrics

Abstract Individual authentication using artefact metrics has received increasing attention, as greater importance has been placed on the security of individual information. These artefact metrics must satisfy the requirements of individuality, measurement stability, durability, and clone resistance...

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Main Authors: Shunya Ito, Toshiyuki Omori, Masao Ando, Hiroyuki Yamazaki, Masaru Nakagawa
Format: Article
Language:English
Published: Nature Publishing Group 2021-08-01
Series:Scientific Reports
Online Access:https://doi.org/10.1038/s41598-021-95953-0
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spelling doaj-e23c4b9d5798415291a98b856fc94e952021-08-22T11:25:54ZengNature Publishing GroupScientific Reports2045-23222021-08-011111910.1038/s41598-021-95953-0Plastic deformation of synthetic quartz nanopillars by nanoindentation for multi-scale and multi-level security artefact metricsShunya Ito0Toshiyuki Omori1Masao Ando2Hiroyuki Yamazaki3Masaru Nakagawa4Institute of Multidisciplinary Research for Advanced Materials (IMRAM), Tohoku UniversityInstitute of Multidisciplinary Research for Advanced Materials (IMRAM), Tohoku UniversitySpecialty Chemicals Research Center, Shin-Etsu Chemical Co., Ltd.Specialty Chemicals Research Center, Shin-Etsu Chemical Co., Ltd.Institute of Multidisciplinary Research for Advanced Materials (IMRAM), Tohoku UniversityAbstract Individual authentication using artefact metrics has received increasing attention, as greater importance has been placed on the security of individual information. These artefact metrics must satisfy the requirements of individuality, measurement stability, durability, and clone resistance, in addition to possessing unique physical features. In this study, we proposed that nanostructures of synthetic quartz (SQ) deposited on an SQ plate may provide sophisticated artefact metrics if morphological changes could be intentionally introduced into the SQ nanostructures at certain positions. We fabricated SQ nanopillars using a mass-production method (ultraviolet nanoimprint lithography) and investigated their mechanical deformation using nanoindentation with a spheroid diamond tip through a loading and unloading cycle. The SQ nanopillars with an aspect ratio of 1 (i.e., diameters D of 100 and 200 nm with corresponding heights H of 100 and 200 nm, respectively) could be plastically deformed without collapsing within a specified pillar-array format at programmed positions. The plastically deformed SQ nanopillar arrays demonstrated multi-scale (sub-millimetre, micrometre, and nanometre) and multi-level (shape, area, diameter, and height) individuality authentication and clone resistance. Because SQ is physically and chemically stable and durable, individuality authentication can be a highly reliable tool on Earth and in space.https://doi.org/10.1038/s41598-021-95953-0
collection DOAJ
language English
format Article
sources DOAJ
author Shunya Ito
Toshiyuki Omori
Masao Ando
Hiroyuki Yamazaki
Masaru Nakagawa
spellingShingle Shunya Ito
Toshiyuki Omori
Masao Ando
Hiroyuki Yamazaki
Masaru Nakagawa
Plastic deformation of synthetic quartz nanopillars by nanoindentation for multi-scale and multi-level security artefact metrics
Scientific Reports
author_facet Shunya Ito
Toshiyuki Omori
Masao Ando
Hiroyuki Yamazaki
Masaru Nakagawa
author_sort Shunya Ito
title Plastic deformation of synthetic quartz nanopillars by nanoindentation for multi-scale and multi-level security artefact metrics
title_short Plastic deformation of synthetic quartz nanopillars by nanoindentation for multi-scale and multi-level security artefact metrics
title_full Plastic deformation of synthetic quartz nanopillars by nanoindentation for multi-scale and multi-level security artefact metrics
title_fullStr Plastic deformation of synthetic quartz nanopillars by nanoindentation for multi-scale and multi-level security artefact metrics
title_full_unstemmed Plastic deformation of synthetic quartz nanopillars by nanoindentation for multi-scale and multi-level security artefact metrics
title_sort plastic deformation of synthetic quartz nanopillars by nanoindentation for multi-scale and multi-level security artefact metrics
publisher Nature Publishing Group
series Scientific Reports
issn 2045-2322
publishDate 2021-08-01
description Abstract Individual authentication using artefact metrics has received increasing attention, as greater importance has been placed on the security of individual information. These artefact metrics must satisfy the requirements of individuality, measurement stability, durability, and clone resistance, in addition to possessing unique physical features. In this study, we proposed that nanostructures of synthetic quartz (SQ) deposited on an SQ plate may provide sophisticated artefact metrics if morphological changes could be intentionally introduced into the SQ nanostructures at certain positions. We fabricated SQ nanopillars using a mass-production method (ultraviolet nanoimprint lithography) and investigated their mechanical deformation using nanoindentation with a spheroid diamond tip through a loading and unloading cycle. The SQ nanopillars with an aspect ratio of 1 (i.e., diameters D of 100 and 200 nm with corresponding heights H of 100 and 200 nm, respectively) could be plastically deformed without collapsing within a specified pillar-array format at programmed positions. The plastically deformed SQ nanopillar arrays demonstrated multi-scale (sub-millimetre, micrometre, and nanometre) and multi-level (shape, area, diameter, and height) individuality authentication and clone resistance. Because SQ is physically and chemically stable and durable, individuality authentication can be a highly reliable tool on Earth and in space.
url https://doi.org/10.1038/s41598-021-95953-0
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