5-Methyl-N′-(5-methyl-1-phenyl-1H-1,2,3-triazole-4-carbonyl)-1-phenyl-1H-1,2,3-triazole-4-carbohydrazide
The asymmetric unit of the title compound, C20H18N8O2, comprises one complete molecule and a half molecule completed by crystallographic twofold symmetry leading to Z = 12. The dihedral angles between the planes of the linked phenyl and methyltriazolyl groups are 69.48 (5) and 44.85 (9)° for the fir...
| Main Authors: | , , , , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
International Union of Crystallography
2018-03-01
|
| Series: | IUCrData |
| Subjects: | |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S2414314618004248 |
| id |
doaj-e22ba49f692147908604e2fa91f1ef6b |
|---|---|
| record_format |
Article |
| spelling |
doaj-e22ba49f692147908604e2fa91f1ef6b2020-11-24T22:53:45ZengInternational Union of CrystallographyIUCrData2414-31462018-03-0133x18042410.1107/S2414314618004248hb42155-Methyl-N′-(5-methyl-1-phenyl-1H-1,2,3-triazole-4-carbonyl)-1-phenyl-1H-1,2,3-triazole-4-carbohydrazideGamal A. El-Hiti0Bakr F. Abdel-Wahab1Mohamed S. Mostafa2Rizk E. Khidre3Amany S. Hegazy4Benson M. Kariuki5Cornea Research Chair, Department of Optometry, College of Applied Medical Sciences, King Saud University, PO Box 10219, Riyadh 11433, Saudi ArabiaDepartment of Chemistry, College of Science and Humanities, Shaqra University, Duwadimi, Saudi ArabiaChemistry Department, Faculty of Science, Damietta University, EgyptChemistry Department, Faculty of Science, Jazan University, Jazan 2079, Saudi ArabiaSchool of Chemistry, Cardiff University, Main Building, Park Place, Cardiff CF10 3AT, UKSchool of Chemistry, Cardiff University, Main Building, Park Place, Cardiff CF10 3AT, UKThe asymmetric unit of the title compound, C20H18N8O2, comprises one complete molecule and a half molecule completed by crystallographic twofold symmetry leading to Z = 12. The dihedral angles between the planes of the linked phenyl and methyltriazolyl groups are 69.48 (5) and 44.85 (9)° for the first molecule and 42.88 (9)° for the second. The conformations of the diformyl hydrazyl groups of the molecules are similar as indicated by C—N—N—C torsion angles of −83.4 (2) and −86.4 (3)°. In the crystal, neighbouring molecules are linked by pairs of N—H...O hydrogen bonds to form independent columns propagating parallel to the c-axis direction.http://scripts.iucr.org/cgi-bin/paper?S2414314618004248crystal structure1,2,3-triazolecarbohydrazide |
| collection |
DOAJ |
| language |
English |
| format |
Article |
| sources |
DOAJ |
| author |
Gamal A. El-Hiti Bakr F. Abdel-Wahab Mohamed S. Mostafa Rizk E. Khidre Amany S. Hegazy Benson M. Kariuki |
| spellingShingle |
Gamal A. El-Hiti Bakr F. Abdel-Wahab Mohamed S. Mostafa Rizk E. Khidre Amany S. Hegazy Benson M. Kariuki 5-Methyl-N′-(5-methyl-1-phenyl-1H-1,2,3-triazole-4-carbonyl)-1-phenyl-1H-1,2,3-triazole-4-carbohydrazide IUCrData crystal structure 1,2,3-triazole carbohydrazide |
| author_facet |
Gamal A. El-Hiti Bakr F. Abdel-Wahab Mohamed S. Mostafa Rizk E. Khidre Amany S. Hegazy Benson M. Kariuki |
| author_sort |
Gamal A. El-Hiti |
| title |
5-Methyl-N′-(5-methyl-1-phenyl-1H-1,2,3-triazole-4-carbonyl)-1-phenyl-1H-1,2,3-triazole-4-carbohydrazide |
| title_short |
5-Methyl-N′-(5-methyl-1-phenyl-1H-1,2,3-triazole-4-carbonyl)-1-phenyl-1H-1,2,3-triazole-4-carbohydrazide |
| title_full |
5-Methyl-N′-(5-methyl-1-phenyl-1H-1,2,3-triazole-4-carbonyl)-1-phenyl-1H-1,2,3-triazole-4-carbohydrazide |
| title_fullStr |
5-Methyl-N′-(5-methyl-1-phenyl-1H-1,2,3-triazole-4-carbonyl)-1-phenyl-1H-1,2,3-triazole-4-carbohydrazide |
| title_full_unstemmed |
5-Methyl-N′-(5-methyl-1-phenyl-1H-1,2,3-triazole-4-carbonyl)-1-phenyl-1H-1,2,3-triazole-4-carbohydrazide |
| title_sort |
5-methyl-n′-(5-methyl-1-phenyl-1h-1,2,3-triazole-4-carbonyl)-1-phenyl-1h-1,2,3-triazole-4-carbohydrazide |
| publisher |
International Union of Crystallography |
| series |
IUCrData |
| issn |
2414-3146 |
| publishDate |
2018-03-01 |
| description |
The asymmetric unit of the title compound, C20H18N8O2, comprises one complete molecule and a half molecule completed by crystallographic twofold symmetry leading to Z = 12. The dihedral angles between the planes of the linked phenyl and methyltriazolyl groups are 69.48 (5) and 44.85 (9)° for the first molecule and 42.88 (9)° for the second. The conformations of the diformyl hydrazyl groups of the molecules are similar as indicated by C—N—N—C torsion angles of −83.4 (2) and −86.4 (3)°. In the crystal, neighbouring molecules are linked by pairs of N—H...O hydrogen bonds to form independent columns propagating parallel to the c-axis direction. |
| topic |
crystal structure 1,2,3-triazole carbohydrazide |
| url |
http://scripts.iucr.org/cgi-bin/paper?S2414314618004248 |
| work_keys_str_mv |
AT gamalaelhiti 5methyln5methyl1phenyl1h123triazole4carbonyl1phenyl1h123triazole4carbohydrazide AT bakrfabdelwahab 5methyln5methyl1phenyl1h123triazole4carbonyl1phenyl1h123triazole4carbohydrazide AT mohamedsmostafa 5methyln5methyl1phenyl1h123triazole4carbonyl1phenyl1h123triazole4carbohydrazide AT rizkekhidre 5methyln5methyl1phenyl1h123triazole4carbonyl1phenyl1h123triazole4carbohydrazide AT amanyshegazy 5methyln5methyl1phenyl1h123triazole4carbonyl1phenyl1h123triazole4carbohydrazide AT bensonmkariuki 5methyln5methyl1phenyl1h123triazole4carbonyl1phenyl1h123triazole4carbohydrazide |
| _version_ |
1725662041463586816 |