Effect of surfactant concentration on the morphology of MoxSy nanoparticles prepared by a solvothermal route

The preparation of MoxSy nanoparticles with different morphologies via a surfactant-assisted one-pot solvothermal route was reported. The concentration of surfactant was studied to evaluate its effects on the morphology and the size of the as obtained nanoparticles. The final products were comprehen...

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Main Authors: Akram Hanane, Mateos-Pedrero Cecilia, Gallegos-Suarez Esteban, Chafik Tarik, Guerrero-Ruiz Antonio, Rodríguez-Ramos Inmaculada
Format: Article
Language:English
Published: De Gruyter 2017-04-01
Series:Green Processing and Synthesis
Subjects:
Online Access:https://doi.org/10.1515/gps-2016-0045
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spelling doaj-e1f0480fc9c14954bc0a4373fb2e05982021-10-02T19:17:01ZengDe GruyterGreen Processing and Synthesis2191-95422191-95502017-04-016216117110.1515/gps-2016-0045Effect of surfactant concentration on the morphology of MoxSy nanoparticles prepared by a solvothermal routeAkram Hanane0Mateos-Pedrero Cecilia1Gallegos-Suarez Esteban2Chafik Tarik3Guerrero-Ruiz Antonio4Rodríguez-Ramos Inmaculada5Instituto de Catálisis y Petroleoquímica, CSIC, and Grupo de diseño y aplicación de catalizadores heterogéneos UA UNED- ICP (CSIC), Marie Curie 2, 28049 Madrid, SpainLaboratory for Process Engineering, Environment, Biotechnology and Energy, Faculdade de Engenhariada, Universidade do Porto Rua Roberto Frias, s/n4200-465 Porto, PortugalInstituto de Catálisis y Petroleoquímica, CSIC, and Grupo de diseño y aplicación de catalizadores heterogéneos UA UNED- ICP (CSIC), Marie Curie 2, 28049 Madrid, SpainLaboratory LGCVR, Faculty of Sciences and Techniques of Tangier, University Abdelmalek Essâadi, B.P. 416 Tangier, MoroccoInstituto de Catálisis y Petroleoquímica, CSIC, and Grupo de diseño y aplicación de catalizadores heterogéneos UA UNED- ICP (CSIC), Marie Curie 2, 28049 Madrid, SpainInstituto de Catálisis y Petroleoquímica, CSIC, and Grupo de diseño y aplicación de catalizadores heterogéneos UA UNED- ICP (CSIC), Marie Curie 2, 28049 Madrid, SpainThe preparation of MoxSy nanoparticles with different morphologies via a surfactant-assisted one-pot solvothermal route was reported. The concentration of surfactant was studied to evaluate its effects on the morphology and the size of the as obtained nanoparticles. The final products were comprehensively characterized using XRD, TEM, HRTEM, IR, TGA and XPS. It was found that at low surfactant concentration, MoS2 spherical shapes were obtained whereas tubular morphologies are formed at higher concentration. This issue has been discussed based on various relevant experimental data.https://doi.org/10.1515/gps-2016-0045mos2nanospheresnanotubessolvothermal synthesissurfactant
collection DOAJ
language English
format Article
sources DOAJ
author Akram Hanane
Mateos-Pedrero Cecilia
Gallegos-Suarez Esteban
Chafik Tarik
Guerrero-Ruiz Antonio
Rodríguez-Ramos Inmaculada
spellingShingle Akram Hanane
Mateos-Pedrero Cecilia
Gallegos-Suarez Esteban
Chafik Tarik
Guerrero-Ruiz Antonio
Rodríguez-Ramos Inmaculada
Effect of surfactant concentration on the morphology of MoxSy nanoparticles prepared by a solvothermal route
Green Processing and Synthesis
mos2
nanospheres
nanotubes
solvothermal synthesis
surfactant
author_facet Akram Hanane
Mateos-Pedrero Cecilia
Gallegos-Suarez Esteban
Chafik Tarik
Guerrero-Ruiz Antonio
Rodríguez-Ramos Inmaculada
author_sort Akram Hanane
title Effect of surfactant concentration on the morphology of MoxSy nanoparticles prepared by a solvothermal route
title_short Effect of surfactant concentration on the morphology of MoxSy nanoparticles prepared by a solvothermal route
title_full Effect of surfactant concentration on the morphology of MoxSy nanoparticles prepared by a solvothermal route
title_fullStr Effect of surfactant concentration on the morphology of MoxSy nanoparticles prepared by a solvothermal route
title_full_unstemmed Effect of surfactant concentration on the morphology of MoxSy nanoparticles prepared by a solvothermal route
title_sort effect of surfactant concentration on the morphology of moxsy nanoparticles prepared by a solvothermal route
publisher De Gruyter
series Green Processing and Synthesis
issn 2191-9542
2191-9550
publishDate 2017-04-01
description The preparation of MoxSy nanoparticles with different morphologies via a surfactant-assisted one-pot solvothermal route was reported. The concentration of surfactant was studied to evaluate its effects on the morphology and the size of the as obtained nanoparticles. The final products were comprehensively characterized using XRD, TEM, HRTEM, IR, TGA and XPS. It was found that at low surfactant concentration, MoS2 spherical shapes were obtained whereas tubular morphologies are formed at higher concentration. This issue has been discussed based on various relevant experimental data.
topic mos2
nanospheres
nanotubes
solvothermal synthesis
surfactant
url https://doi.org/10.1515/gps-2016-0045
work_keys_str_mv AT akramhanane effectofsurfactantconcentrationonthemorphologyofmoxsynanoparticlespreparedbyasolvothermalroute
AT mateospedrerocecilia effectofsurfactantconcentrationonthemorphologyofmoxsynanoparticlespreparedbyasolvothermalroute
AT gallegossuarezesteban effectofsurfactantconcentrationonthemorphologyofmoxsynanoparticlespreparedbyasolvothermalroute
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AT guerreroruizantonio effectofsurfactantconcentrationonthemorphologyofmoxsynanoparticlespreparedbyasolvothermalroute
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