Optimization of reaction parameters for the green synthesis of zero valent iron nanoparticles using pine tree needles

In the current study, the optimal reaction condition for fabrication of INPs by using pine tree (Pinus eldarica) leaf extract was developed. A fractional factorial design was utilized to screen the effective parameters in the green synthesis reaction, and central composite face design was employed t...

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Main Authors:	Kheshtzar Raziyeh, Berenjian Aydin, Taghizadeh Seyedeh-Masoumeh, Ghasemi Younes, Asad Ali Ghanbari, Ebrahiminezhad Alireza
Format:	Article
Language:	English
Published:	De Gruyter 2019-01-01
Series:	Green Processing and Synthesis
Subjects:	biosynthesis design of experiments (doe) plant mediated synthesis optimization response surface methodology (rsm)
Online Access:	https://doi.org/10.1515/gps-2019-0055

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spelling	doaj-dfb0151e06e84612a285c241985a7f262021-10-02T17:48:06ZengDe GruyterGreen Processing and Synthesis2191-95502019-01-018184685510.1515/gps-2019-0055gps-2019-0055Optimization of reaction parameters for the green synthesis of zero valent iron nanoparticles using pine tree needlesKheshtzar Raziyeh0Berenjian Aydin1Taghizadeh Seyedeh-Masoumeh2Ghasemi Younes3Asad Ali Ghanbari4Ebrahiminezhad Alireza5Department of Pharmaceutical Biotechnology, School of Pharmacy and Pharmaceutical Sciences Research Center, Shiraz University of Medical Sciences, Shiraz, IranSchool of Engineering, Faculty of Science and Engineering, University of Waikato, Hamilton, New ZealandDepartment of Medical Biotechnology, School of Medicine, and Noncommunicable Disease Research Centre, Fasa University of Medical Sciences, Fasa, IranDepartment of Pharmaceutical Biotechnology, School of Pharmacy and Pharmaceutical Sciences Research Center, Shiraz University of Medical Sciences, Shiraz, IranDepartment of Medical Biotechnology, School of Medicine, and Noncommunicable Disease Research Centre, Fasa University of Medical Sciences, Fasa, IranDepartment of Medical Nanotechnology, School of Advanced Medical Sciences and Technologies, Shiraz University of Medical Sciences, Shiraz, IranIn the current study, the optimal reaction condition for fabrication of INPs by using pine tree (Pinus eldarica) leaf extract was developed. A fractional factorial design was utilized to screen the effective parameters in the green synthesis reaction, and central composite face design was employed to achieve the optimal reaction condition. Leaf extract and iron precursor concentrations were found to be the most effective parameters for the fabrication of INPs. Physicochemical characteristics of the obtained nanoparticles were evaluated by transmission electron microscopy (TEM), Fourier transform infrared (FTIR) spectroscopy, X-ray diffractometer (XRD), vibrating sample magnetometer (VSM), thermogravimetric analysis (TGA), and derivative thermo gravimetric (DTG). The prepared particles were found to be zero-valent iron nanoparticles without any iron oxide impurities. Nanoparticles were spherical in shape with diameters ranging from 8 nm to 34 nm with a mean particle size of 18 nm. The fabricated particles were amorphous with a low magnetization value of 33 memu/g.https://doi.org/10.1515/gps-2019-0055biosynthesisdesign of experiments (doe)plant mediated synthesisoptimizationresponse surface methodology (rsm)
collection	DOAJ
language	English
format	Article
sources	DOAJ
author	Kheshtzar Raziyeh Berenjian Aydin Taghizadeh Seyedeh-Masoumeh Ghasemi Younes Asad Ali Ghanbari Ebrahiminezhad Alireza
spellingShingle	Kheshtzar Raziyeh Berenjian Aydin Taghizadeh Seyedeh-Masoumeh Ghasemi Younes Asad Ali Ghanbari Ebrahiminezhad Alireza Optimization of reaction parameters for the green synthesis of zero valent iron nanoparticles using pine tree needles Green Processing and Synthesis biosynthesis design of experiments (doe) plant mediated synthesis optimization response surface methodology (rsm)
author_facet	Kheshtzar Raziyeh Berenjian Aydin Taghizadeh Seyedeh-Masoumeh Ghasemi Younes Asad Ali Ghanbari Ebrahiminezhad Alireza
author_sort	Kheshtzar Raziyeh
title	Optimization of reaction parameters for the green synthesis of zero valent iron nanoparticles using pine tree needles
title_short	Optimization of reaction parameters for the green synthesis of zero valent iron nanoparticles using pine tree needles
title_full	Optimization of reaction parameters for the green synthesis of zero valent iron nanoparticles using pine tree needles
title_fullStr	Optimization of reaction parameters for the green synthesis of zero valent iron nanoparticles using pine tree needles
title_full_unstemmed	Optimization of reaction parameters for the green synthesis of zero valent iron nanoparticles using pine tree needles
title_sort	optimization of reaction parameters for the green synthesis of zero valent iron nanoparticles using pine tree needles
publisher	De Gruyter
series	Green Processing and Synthesis
issn	2191-9550
publishDate	2019-01-01
description	In the current study, the optimal reaction condition for fabrication of INPs by using pine tree (Pinus eldarica) leaf extract was developed. A fractional factorial design was utilized to screen the effective parameters in the green synthesis reaction, and central composite face design was employed to achieve the optimal reaction condition. Leaf extract and iron precursor concentrations were found to be the most effective parameters for the fabrication of INPs. Physicochemical characteristics of the obtained nanoparticles were evaluated by transmission electron microscopy (TEM), Fourier transform infrared (FTIR) spectroscopy, X-ray diffractometer (XRD), vibrating sample magnetometer (VSM), thermogravimetric analysis (TGA), and derivative thermo gravimetric (DTG). The prepared particles were found to be zero-valent iron nanoparticles without any iron oxide impurities. Nanoparticles were spherical in shape with diameters ranging from 8 nm to 34 nm with a mean particle size of 18 nm. The fabricated particles were amorphous with a low magnetization value of 33 memu/g.
topic	biosynthesis design of experiments (doe) plant mediated synthesis optimization response surface methodology (rsm)
url	https://doi.org/10.1515/gps-2019-0055
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Optimization of reaction parameters for the green synthesis of zero valent iron nanoparticles using pine tree needles

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