N-(3-Bromophenyl)-3,4,5-trimethoxybenzamide

In the title compound, C16H16BrNO4, the dihedral between the planes of the aromatic rings is 7.74 (18)°. The amide group is tilted with respect to the bromo- and methoxy-substituted aromatic rings by 36.3 (8) and 35.2 (8)°, respecti...

Full description

Bibliographic Details
Main Authors: Aamer Saeed, Shahid Hussain, Aliya Ibrar, Michael Bolte
Format: Article
Language:English
Published: International Union of Crystallography 2009-07-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536809020509
Description
Summary:In the title compound, C16H16BrNO4, the dihedral between the planes of the aromatic rings is 7.74 (18)°. The amide group is tilted with respect to the bromo- and methoxy-substituted aromatic rings by 36.3 (8) and 35.2 (8)°, respectively. The meta-methoxy groups are essentially in-plane with the aromatic ring [dihedral angles CH3—O—C—C = −4.6 (4) and −2.5 (4)°]. The para-methoxy group is markedly displaced from the ring plane [dihedral angle CH3—O—C—C = −72.5 (4)°]. The crystal packing is stabilized by N—H...O hydrogen bonds linking the molecules into chains running along the b axis.
ISSN:1600-5368