Evaluation of acid digestion techniques to estimate chromium contents in cattle feces

The objective of this work was to evaluate the accuracy of digestion techniques using nitric and perchloric acid at the ratios of 2:1, 3:1, and 4:1 v v-1, in one- or two-step digestion, to estimate chromium contents in cattle feces, using sodium molybdate as a catalyst. Fecal standards containing kn...

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Bibliographic Details
Main Authors: Gabriel Cipriano Rocha, Malber Nathan Nobre Palma, Edenio Detmann, Sebastião de Campos Valadares Filho
Format: Article
Language:English
Published: Embrapa Informação Tecnológica 2015-01-01
Series:Pesquisa Agropecuária Brasileira
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Online Access:http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-204X2015000100092&lng=en&tlng=en
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Summary:The objective of this work was to evaluate the accuracy of digestion techniques using nitric and perchloric acid at the ratios of 2:1, 3:1, and 4:1 v v-1, in one- or two-step digestion, to estimate chromium contents in cattle feces, using sodium molybdate as a catalyst. Fecal standards containing known chromium contents (0, 2, 4, 6, 8, and 10 g kg-1) were produced from feces of five animals. The chromium content in cattle feces is accurately estimated using digestion techniques based on nitric and perchloric acids, at a 3:1 v v-1 ratio, in one-step digestion, with sodium molybdate as a catalyst.
ISSN:1678-3921