Assignments of NMR Spectral Data of a Novel Carbazole-Triazinoindole Based N-Acylhydrazone Derivative

N-acylhydrazone compounds have two isomers, E/cis and E/trans, in polar solvents. In this work, 1H and 13C nuclear magnetic resonance (NMR) signals, coupling constants (J), and the spatial structures of the two isomers (E/cis and E/trans) of a novel carbazole-triazinoindole based N-acylhydrazone der...

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Main Authors:	LI Ying-jun, YANG Hong-jing, LIU Ji-hong, JIN Kun, LIN Le-di, LIU Xue-jie
Format:	Article
Language:	zho
Published:	Science Press 2020-12-01
Series:	Chinese Journal of Magnetic Resonance
Subjects:	nuclear magnetic resonance (nmr) assignment 2d nmr carbazole-triazinoindole n-acylhydrazone derivative
Online Access:	http://121.43.60.238/bpxzz/EN/10.11938/cjmr20202803

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spelling	doaj-d38dbd9bcf374bcbb89f62674e22261f2021-03-03T08:14:48ZzhoScience PressChinese Journal of Magnetic Resonance1000-45561000-45562020-12-01370449650410.11938/cjmr20202803Assignments of NMR Spectral Data of a Novel Carbazole-Triazinoindole Based N-Acylhydrazone DerivativeLI Ying-jun0YANG Hong-jing1LIU Ji-hong2JIN Kun3LIN Le-di4LIU Xue-jie5College of Chemistry and Chemical Engineering, Liaoning Normal University, Dalian 116029, ChinaCollege of Chemistry and Chemical Engineering, Liaoning Normal University, Dalian 116029, ChinaChemistry Analysis and Inspection Center, Dalian University of Technology, Dalian 116024, China State Key Laboratory of Fine Chemicals, Dalian University of Technology, Dalian 116023, ChinaCollege of Chemistry and Chemical Engineering, Liaoning Normal University, Dalian 116029, ChinaCollege of Chemistry and Chemical Engineering, Liaoning Normal University, Dalian 116029, ChinaN-acylhydrazone compounds have two isomers, E/cis and E/trans, in polar solvents. In this work, 1H and 13C nuclear magnetic resonance (NMR) signals, coupling constants (J), and the spatial structures of the two isomers (E/cis and E/trans) of a novel carbazole-triazinoindole based N-acylhydrazone derivative 3, 2-(5H-[1,2,4] triazine[5,6-b]indol-3-ylthio)-N'-(9-ethylcarbazol-3-ylmethylene)acetylhydrazine, were obtained by one-dimensional and two-dimensional NMR techniques, infrared spectroscopy (IR) and elemental analysis. The ratios of the two isomers were determined.http://121.43.60.238/bpxzz/EN/10.11938/cjmr20202803nuclear magnetic resonance (nmr)assignment2d nmrcarbazole-triazinoindolen-acylhydrazone derivative
collection	DOAJ
language	zho
format	Article
sources	DOAJ
author	LI Ying-jun YANG Hong-jing LIU Ji-hong JIN Kun LIN Le-di LIU Xue-jie
spellingShingle	LI Ying-jun YANG Hong-jing LIU Ji-hong JIN Kun LIN Le-di LIU Xue-jie Assignments of NMR Spectral Data of a Novel Carbazole-Triazinoindole Based N-Acylhydrazone Derivative Chinese Journal of Magnetic Resonance nuclear magnetic resonance (nmr) assignment 2d nmr carbazole-triazinoindole n-acylhydrazone derivative
author_facet	LI Ying-jun YANG Hong-jing LIU Ji-hong JIN Kun LIN Le-di LIU Xue-jie
author_sort	LI Ying-jun
title	Assignments of NMR Spectral Data of a Novel Carbazole-Triazinoindole Based N-Acylhydrazone Derivative
title_short	Assignments of NMR Spectral Data of a Novel Carbazole-Triazinoindole Based N-Acylhydrazone Derivative
title_full	Assignments of NMR Spectral Data of a Novel Carbazole-Triazinoindole Based N-Acylhydrazone Derivative
title_fullStr	Assignments of NMR Spectral Data of a Novel Carbazole-Triazinoindole Based N-Acylhydrazone Derivative
title_full_unstemmed	Assignments of NMR Spectral Data of a Novel Carbazole-Triazinoindole Based N-Acylhydrazone Derivative
title_sort	assignments of nmr spectral data of a novel carbazole-triazinoindole based n-acylhydrazone derivative
publisher	Science Press
series	Chinese Journal of Magnetic Resonance
issn	1000-4556 1000-4556
publishDate	2020-12-01
description	N-acylhydrazone compounds have two isomers, E/cis and E/trans, in polar solvents. In this work, 1H and 13C nuclear magnetic resonance (NMR) signals, coupling constants (J), and the spatial structures of the two isomers (E/cis and E/trans) of a novel carbazole-triazinoindole based N-acylhydrazone derivative 3, 2-(5H-[1,2,4] triazine[5,6-b]indol-3-ylthio)-N'-(9-ethylcarbazol-3-ylmethylene)acetylhydrazine, were obtained by one-dimensional and two-dimensional NMR techniques, infrared spectroscopy (IR) and elemental analysis. The ratios of the two isomers were determined.
topic	nuclear magnetic resonance (nmr) assignment 2d nmr carbazole-triazinoindole n-acylhydrazone derivative
url	http://121.43.60.238/bpxzz/EN/10.11938/cjmr20202803
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Assignments of NMR Spectral Data of a Novel Carbazole-Triazinoindole Based N-Acylhydrazone Derivative

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