10,10'-Dimethoxy-9,9'-biazuleno[2,1-c]phenanthrene

The title compound was prepared by the regioselective homocoupling of 10-methoxyazuleno[2,1-c]phenanthrene in the presence of ammonium persulfate. The structure of the synthesized compound was assigned on the basis of its 1H-NMR, FT-IR, and mass spectral data. Its crystal structure and electrochemi...

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Main Authors: Kosuke Yamamoto, Ryota Nakamae, Hiroshi Suemune, Kazuteru Usui
Format: Article
Language:English
Published: MDPI AG 2015-02-01
Series:Molbank
Subjects:
Online Access:http://www.mdpi.com/1422-8599/2015/1/M843
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spelling doaj-d2afc041c01e4c5db215c7a9eb4458612020-11-24T22:58:07ZengMDPI AGMolbank1422-85992015-02-0120151M84310.3390/M843M84310,10'-Dimethoxy-9,9'-biazuleno[2,1-c]phenanthreneKosuke Yamamoto0Ryota Nakamae1Hiroshi Suemune2Kazuteru Usui3Graduate School of Pharmaceutical Sciences, Kyushu University, 3-1-1 Maidashi, Higashi-ku, Fukuoka 812-8582, JapanGraduate School of Pharmaceutical Sciences, Kyushu University, 3-1-1 Maidashi, Higashi-ku, Fukuoka 812-8582, JapanGraduate School of Pharmaceutical Sciences, Kyushu University, 3-1-1 Maidashi, Higashi-ku, Fukuoka 812-8582, JapanGraduate School of Pharmaceutical Sciences, Kyushu University, 3-1-1 Maidashi, Higashi-ku, Fukuoka 812-8582, JapanThe title compound was prepared by the regioselective homocoupling of 10-methoxyazuleno[2,1-c]phenanthrene in the presence of ammonium persulfate. The structure of the synthesized compound was assigned on the basis of its 1H-NMR, FT-IR, and mass spectral data. Its crystal structure and electrochemical properties are also reported.http://www.mdpi.com/1422-8599/2015/1/M843azulene-fused helicenehomocoupling reactionammonium persulfate
collection DOAJ
language English
format Article
sources DOAJ
author Kosuke Yamamoto
Ryota Nakamae
Hiroshi Suemune
Kazuteru Usui
spellingShingle Kosuke Yamamoto
Ryota Nakamae
Hiroshi Suemune
Kazuteru Usui
10,10'-Dimethoxy-9,9'-biazuleno[2,1-c]phenanthrene
Molbank
azulene-fused helicene
homocoupling reaction
ammonium persulfate
author_facet Kosuke Yamamoto
Ryota Nakamae
Hiroshi Suemune
Kazuteru Usui
author_sort Kosuke Yamamoto
title 10,10'-Dimethoxy-9,9'-biazuleno[2,1-c]phenanthrene
title_short 10,10'-Dimethoxy-9,9'-biazuleno[2,1-c]phenanthrene
title_full 10,10'-Dimethoxy-9,9'-biazuleno[2,1-c]phenanthrene
title_fullStr 10,10'-Dimethoxy-9,9'-biazuleno[2,1-c]phenanthrene
title_full_unstemmed 10,10'-Dimethoxy-9,9'-biazuleno[2,1-c]phenanthrene
title_sort 10,10'-dimethoxy-9,9'-biazuleno[2,1-c]phenanthrene
publisher MDPI AG
series Molbank
issn 1422-8599
publishDate 2015-02-01
description The title compound was prepared by the regioselective homocoupling of 10-methoxyazuleno[2,1-c]phenanthrene in the presence of ammonium persulfate. The structure of the synthesized compound was assigned on the basis of its 1H-NMR, FT-IR, and mass spectral data. Its crystal structure and electrochemical properties are also reported.
topic azulene-fused helicene
homocoupling reaction
ammonium persulfate
url http://www.mdpi.com/1422-8599/2015/1/M843
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AT ryotanakamae 1010dimethoxy99biazuleno21cphenanthrene
AT hiroshisuemune 1010dimethoxy99biazuleno21cphenanthrene
AT kazuteruusui 1010dimethoxy99biazuleno21cphenanthrene
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