10,10'-Dimethoxy-9,9'-biazuleno[2,1-c]phenanthrene
The title compound was prepared by the regioselective homocoupling of 10-methoxyazuleno[2,1-c]phenanthrene in the presence of ammonium persulfate. The structure of the synthesized compound was assigned on the basis of its 1H-NMR, FT-IR, and mass spectral data. Its crystal structure and electrochemi...
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2015-02-01
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Online Access: | http://www.mdpi.com/1422-8599/2015/1/M843 |
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doaj-d2afc041c01e4c5db215c7a9eb4458612020-11-24T22:58:07ZengMDPI AGMolbank1422-85992015-02-0120151M84310.3390/M843M84310,10'-Dimethoxy-9,9'-biazuleno[2,1-c]phenanthreneKosuke Yamamoto0Ryota Nakamae1Hiroshi Suemune2Kazuteru Usui3Graduate School of Pharmaceutical Sciences, Kyushu University, 3-1-1 Maidashi, Higashi-ku, Fukuoka 812-8582, JapanGraduate School of Pharmaceutical Sciences, Kyushu University, 3-1-1 Maidashi, Higashi-ku, Fukuoka 812-8582, JapanGraduate School of Pharmaceutical Sciences, Kyushu University, 3-1-1 Maidashi, Higashi-ku, Fukuoka 812-8582, JapanGraduate School of Pharmaceutical Sciences, Kyushu University, 3-1-1 Maidashi, Higashi-ku, Fukuoka 812-8582, JapanThe title compound was prepared by the regioselective homocoupling of 10-methoxyazuleno[2,1-c]phenanthrene in the presence of ammonium persulfate. The structure of the synthesized compound was assigned on the basis of its 1H-NMR, FT-IR, and mass spectral data. Its crystal structure and electrochemical properties are also reported.http://www.mdpi.com/1422-8599/2015/1/M843azulene-fused helicenehomocoupling reactionammonium persulfate |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Kosuke Yamamoto Ryota Nakamae Hiroshi Suemune Kazuteru Usui |
spellingShingle |
Kosuke Yamamoto Ryota Nakamae Hiroshi Suemune Kazuteru Usui 10,10'-Dimethoxy-9,9'-biazuleno[2,1-c]phenanthrene Molbank azulene-fused helicene homocoupling reaction ammonium persulfate |
author_facet |
Kosuke Yamamoto Ryota Nakamae Hiroshi Suemune Kazuteru Usui |
author_sort |
Kosuke Yamamoto |
title |
10,10'-Dimethoxy-9,9'-biazuleno[2,1-c]phenanthrene |
title_short |
10,10'-Dimethoxy-9,9'-biazuleno[2,1-c]phenanthrene |
title_full |
10,10'-Dimethoxy-9,9'-biazuleno[2,1-c]phenanthrene |
title_fullStr |
10,10'-Dimethoxy-9,9'-biazuleno[2,1-c]phenanthrene |
title_full_unstemmed |
10,10'-Dimethoxy-9,9'-biazuleno[2,1-c]phenanthrene |
title_sort |
10,10'-dimethoxy-9,9'-biazuleno[2,1-c]phenanthrene |
publisher |
MDPI AG |
series |
Molbank |
issn |
1422-8599 |
publishDate |
2015-02-01 |
description |
The title compound was prepared by the regioselective homocoupling of 10-methoxyazuleno[2,1-c]phenanthrene in the presence of ammonium persulfate. The structure of the synthesized compound was assigned on the basis of its 1H-NMR, FT-IR, and mass spectral data. Its crystal structure and electrochemical properties are also reported. |
topic |
azulene-fused helicene homocoupling reaction ammonium persulfate |
url |
http://www.mdpi.com/1422-8599/2015/1/M843 |
work_keys_str_mv |
AT kosukeyamamoto 1010dimethoxy99biazuleno21cphenanthrene AT ryotanakamae 1010dimethoxy99biazuleno21cphenanthrene AT hiroshisuemune 1010dimethoxy99biazuleno21cphenanthrene AT kazuteruusui 1010dimethoxy99biazuleno21cphenanthrene |
_version_ |
1725648443285700608 |