1-(2-Furoyl)-3-(o-tolyl)thiourea
The title compound, C13H12N2O2S, was synthesized from furoyl isothiocyanate and o-toluidine in dry acetone. The thiourea group is in the thioamide form. The central thiourea fragment makes dihedral angles of 2.6 (1) and 22.4 (1)° with the ketofuran group and the benzene...
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2008-08-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536808020114 |
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doaj-d15d797a116f446385397906237363bd2020-11-25T02:24:30ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682008-08-01648o1414o141410.1107/S16005368080201141-(2-Furoyl)-3-(o-tolyl)thioureaRodrigo S. CorrêaO. Estévez-HernándezJ. DuqueJ. EllenaThe title compound, C13H12N2O2S, was synthesized from furoyl isothiocyanate and o-toluidine in dry acetone. The thiourea group is in the thioamide form. The central thiourea fragment makes dihedral angles of 2.6 (1) and 22.4 (1)° with the ketofuran group and the benzene ring, respectively. The molecular structure is stabilized by N—H...O hydrogen bonds. In the crystal structure, centrosymmetrically related molecules are linked by a pair of N—H...S hydrogen bonds to form a dimer with an R22(6) ring motif.http://scripts.iucr.org/cgi-bin/paper?S1600536808020114 |
| collection |
DOAJ |
| language |
English |
| format |
Article |
| sources |
DOAJ |
| author |
Rodrigo S. Corrêa O. Estévez-Hernández J. Duque J. Ellena |
| spellingShingle |
Rodrigo S. Corrêa O. Estévez-Hernández J. Duque J. Ellena 1-(2-Furoyl)-3-(o-tolyl)thiourea Acta Crystallographica Section E |
| author_facet |
Rodrigo S. Corrêa O. Estévez-Hernández J. Duque J. Ellena |
| author_sort |
Rodrigo S. Corrêa |
| title |
1-(2-Furoyl)-3-(o-tolyl)thiourea |
| title_short |
1-(2-Furoyl)-3-(o-tolyl)thiourea |
| title_full |
1-(2-Furoyl)-3-(o-tolyl)thiourea |
| title_fullStr |
1-(2-Furoyl)-3-(o-tolyl)thiourea |
| title_full_unstemmed |
1-(2-Furoyl)-3-(o-tolyl)thiourea |
| title_sort |
1-(2-furoyl)-3-(o-tolyl)thiourea |
| publisher |
International Union of Crystallography |
| series |
Acta Crystallographica Section E |
| issn |
1600-5368 |
| publishDate |
2008-08-01 |
| description |
The title compound, C13H12N2O2S, was synthesized from furoyl isothiocyanate and o-toluidine in dry acetone. The thiourea group is in the thioamide form. The central thiourea fragment makes dihedral angles of 2.6 (1) and 22.4 (1)° with the ketofuran group and the benzene ring, respectively. The molecular structure is stabilized by N—H...O hydrogen bonds. In the crystal structure, centrosymmetrically related molecules are linked by a pair of N—H...S hydrogen bonds to form a dimer with an R22(6) ring motif. |
| url |
http://scripts.iucr.org/cgi-bin/paper?S1600536808020114 |
| work_keys_str_mv |
AT rodrigoscorr234a 12furoyl3otolylthiourea AT oest233vezhern225ndez 12furoyl3otolylthiourea AT jduque 12furoyl3otolylthiourea AT jellena 12furoyl3otolylthiourea |
| _version_ |
1724855440798384128 |