3-{5-Ethoxycarbonyl-1-[3-(2-oxopyrrolidin-1-yl)propyl]-1H-benzimidazol-2-yl}benzoic acid
In the title compound, C24H25N3O5, the ethoxy group is disordered over two orientations in a 0.853 (14):0.147 (14) ratio. The benzimadazole ring system (r.m.s. deviation = 0.016 Å) makes a dihedral angle of 35.47 (7)° with the attached benzen...
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2013-02-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536813001116 |
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doaj-cfaaa8fafe2f48039f09c3699cd6b5442020-11-24T21:31:44ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682013-02-01692o304o30410.1107/S16005368130011163-{5-Ethoxycarbonyl-1-[3-(2-oxopyrrolidin-1-yl)propyl]-1H-benzimidazol-2-yl}benzoic acidYeong Keng YoonMohamed Ashraf AliSoo Choon TanMohd Mustaqim RosliIbrahim Abdul RazakIn the title compound, C24H25N3O5, the ethoxy group is disordered over two orientations in a 0.853 (14):0.147 (14) ratio. The benzimadazole ring system (r.m.s. deviation = 0.016 Å) makes a dihedral angle of 35.47 (7)° with the attached benzene ring. The pyrrolidine ring adopts an envelope conformation with a methylene C atom as the flap. In the crystal, inversion dimers linked by pairs of O—H...N hydrogen bonds generate R22(16) loops. C—H...O interactions link the dimers into a three-dimensional network.http://scripts.iucr.org/cgi-bin/paper?S1600536813001116 |
| collection |
DOAJ |
| language |
English |
| format |
Article |
| sources |
DOAJ |
| author |
Yeong Keng Yoon Mohamed Ashraf Ali Soo Choon Tan Mohd Mustaqim Rosli Ibrahim Abdul Razak |
| spellingShingle |
Yeong Keng Yoon Mohamed Ashraf Ali Soo Choon Tan Mohd Mustaqim Rosli Ibrahim Abdul Razak 3-{5-Ethoxycarbonyl-1-[3-(2-oxopyrrolidin-1-yl)propyl]-1H-benzimidazol-2-yl}benzoic acid Acta Crystallographica Section E |
| author_facet |
Yeong Keng Yoon Mohamed Ashraf Ali Soo Choon Tan Mohd Mustaqim Rosli Ibrahim Abdul Razak |
| author_sort |
Yeong Keng Yoon |
| title |
3-{5-Ethoxycarbonyl-1-[3-(2-oxopyrrolidin-1-yl)propyl]-1H-benzimidazol-2-yl}benzoic acid |
| title_short |
3-{5-Ethoxycarbonyl-1-[3-(2-oxopyrrolidin-1-yl)propyl]-1H-benzimidazol-2-yl}benzoic acid |
| title_full |
3-{5-Ethoxycarbonyl-1-[3-(2-oxopyrrolidin-1-yl)propyl]-1H-benzimidazol-2-yl}benzoic acid |
| title_fullStr |
3-{5-Ethoxycarbonyl-1-[3-(2-oxopyrrolidin-1-yl)propyl]-1H-benzimidazol-2-yl}benzoic acid |
| title_full_unstemmed |
3-{5-Ethoxycarbonyl-1-[3-(2-oxopyrrolidin-1-yl)propyl]-1H-benzimidazol-2-yl}benzoic acid |
| title_sort |
3-{5-ethoxycarbonyl-1-[3-(2-oxopyrrolidin-1-yl)propyl]-1h-benzimidazol-2-yl}benzoic acid |
| publisher |
International Union of Crystallography |
| series |
Acta Crystallographica Section E |
| issn |
1600-5368 |
| publishDate |
2013-02-01 |
| description |
In the title compound, C24H25N3O5, the ethoxy group is disordered over two orientations in a 0.853 (14):0.147 (14) ratio. The benzimadazole ring system (r.m.s. deviation = 0.016 Å) makes a dihedral angle of 35.47 (7)° with the attached benzene ring. The pyrrolidine ring adopts an envelope conformation with a methylene C atom as the flap. In the crystal, inversion dimers linked by pairs of O—H...N hydrogen bonds generate R22(16) loops. C—H...O interactions link the dimers into a three-dimensional network. |
| url |
http://scripts.iucr.org/cgi-bin/paper?S1600536813001116 |
| work_keys_str_mv |
AT yeongkengyoon 35ethoxycarbonyl132oxopyrrolidin1ylpropyl1hbenzimidazol2ylbenzoicacid AT mohamedashrafali 35ethoxycarbonyl132oxopyrrolidin1ylpropyl1hbenzimidazol2ylbenzoicacid AT soochoontan 35ethoxycarbonyl132oxopyrrolidin1ylpropyl1hbenzimidazol2ylbenzoicacid AT mohdmustaqimrosli 35ethoxycarbonyl132oxopyrrolidin1ylpropyl1hbenzimidazol2ylbenzoicacid AT ibrahimabdulrazak 35ethoxycarbonyl132oxopyrrolidin1ylpropyl1hbenzimidazol2ylbenzoicacid |
| _version_ |
1725960073246670848 |