rac-6-Hydroxy-2,5,7,8-tetramethylchroman-2-carboxamide from synchrotron data

rac-6-Hydroxy-2,5,7,8-tetramethylchroman-2-carboxamide from synchrotron data

The crystal structure of the title water-soluble analogue of vitamin E, trolox amide, C14H19NO3, solved and refined against synchrotron diffraction data, contains two molecules in the asymmetric unit. In both molecules, the heterocyclic ring is in a half-chair conformation. The crystal packing featu...

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Main Authors: Krzysztof Brzezinski, Zbigniew Dauter, Aneta Baj, Piotr Wałejko, Stanisław Witkowski
Format: Article
Language:English
Published: International Union of Crystallography 2011-02-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536811002807
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spelling doaj-cb54dab425284860bddbae5f614f422b2020-11-25T01:52:48ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682011-02-01672o503o50410.1107/S1600536811002807rac-6-Hydroxy-2,5,7,8-tetramethylchroman-2-carboxamide from synchrotron dataKrzysztof BrzezinskiZbigniew DauterAneta BajPiotr WałejkoStanisław WitkowskiThe crystal structure of the title water-soluble analogue of vitamin E, trolox amide, C14H19NO3, solved and refined against synchrotron diffraction data, contains two molecules in the asymmetric unit. In both molecules, the heterocyclic ring is in a half-chair conformation. The crystal packing features a herring-bone pattern generated by N—H...O hydrogen bonds between the hydroxy and amide groups. O—H...O hydrogen bonds also occur. http://scripts.iucr.org/cgi-bin/paper?S1600536811002807
collection DOAJ
language English
format Article
sources DOAJ
author Krzysztof Brzezinski
Zbigniew Dauter
Aneta Baj
Piotr Wałejko
Stanisław Witkowski
spellingShingle Krzysztof Brzezinski
Zbigniew Dauter
Aneta Baj
Piotr Wałejko
Stanisław Witkowski
rac-6-Hydroxy-2,5,7,8-tetramethylchroman-2-carboxamide from synchrotron data
Acta Crystallographica Section E
author_facet Krzysztof Brzezinski
Zbigniew Dauter
Aneta Baj
Piotr Wałejko
Stanisław Witkowski
author_sort Krzysztof Brzezinski
title rac-6-Hydroxy-2,5,7,8-tetramethylchroman-2-carboxamide from synchrotron data
title_short rac-6-Hydroxy-2,5,7,8-tetramethylchroman-2-carboxamide from synchrotron data
title_full rac-6-Hydroxy-2,5,7,8-tetramethylchroman-2-carboxamide from synchrotron data
title_fullStr rac-6-Hydroxy-2,5,7,8-tetramethylchroman-2-carboxamide from synchrotron data
title_full_unstemmed rac-6-Hydroxy-2,5,7,8-tetramethylchroman-2-carboxamide from synchrotron data
title_sort rac-6-hydroxy-2,5,7,8-tetramethylchroman-2-carboxamide from synchrotron data
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2011-02-01
description The crystal structure of the title water-soluble analogue of vitamin E, trolox amide, C14H19NO3, solved and refined against synchrotron diffraction data, contains two molecules in the asymmetric unit. In both molecules, the heterocyclic ring is in a half-chair conformation. The crystal packing features a herring-bone pattern generated by N—H...O hydrogen bonds between the hydroxy and amide groups. O—H...O hydrogen bonds also occur.
url http://scripts.iucr.org/cgi-bin/paper?S1600536811002807
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AT anetabaj rac6hydroxy2578tetramethylchroman2carboxamidefromsynchrotrondata
AT piotrwaamp322ejko rac6hydroxy2578tetramethylchroman2carboxamidefromsynchrotrondata
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