A green HPLC technique with a 100% water mobile phase for detecting imidacloprid and its metabolite 6-chloronicotinic acid
This paper describes a harmless HPLC technique for detecting imidacloprid (ICP) and its metabolite, 6-chloronicotinic acid (6CA), using an isocratic 100 % water mobile phase. Chromatographic separations were performed a Daisopak® SP-200-3-C1-P with water mobile phase and a photodiode-array detector....
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| Format: | Article |
| Language: | English |
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Growing Science
2016-01-01
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| Series: | Current Chemistry Letters |
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| Online Access: | http://www.growingscience.com/ccl/Vol5/ccl_2015_18.pdf |
| Summary: | This paper describes a harmless HPLC technique for detecting imidacloprid (ICP) and its metabolite, 6-chloronicotinic acid (6CA), using an isocratic 100 % water mobile phase. Chromatographic separations were performed a Daisopak® SP-200-3-C1-P with water mobile phase and a photodiode-array detector. The total run time was < 6 min. The system suitability was well within the international acceptance criteria. The detection limits were 0.018 μg/ml for ICP and 0.005 μg/ml for 6CA, respectively. A harmless HPLC method for simultaneous detecting ICP and 6CA was developed and may be further applied to the quantification in animal-derived foods. |
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| ISSN: | 1927-7296 1927-730X |