4-(4-Chlorophenyl)-2,6-bis(1H-indol-3-yl)-1,4-dihydropyridine-3,5-dicarbonitrile ethanol monosolvate

4-(4-Chlorophenyl)-2,6-bis(1H-indol-3-yl)-1,4-dihydropyridine-3,5-dicarbonitrile ethanol monosolvate

In the title compound, C29H18ClN5·C2H6O, the dihydropyridine ring adopts a strongly flattened envelope conformation, with a maximum deviation of 0.139 (2) Å from its best plane for the Csp3 atom. The dihedral angles between the dihydropyridine ri...

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Main Authors: Song-Lei Zhu, Jun-Nian Zheng
Format: Article
Language:English
Published: International Union of Crystallography 2012-05-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536812013906
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spelling doaj-c329681d3cc446ee8401d893bf07e0182020-11-24T21:32:45ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682012-05-01685o1300o130110.1107/S16005368120139064-(4-Chlorophenyl)-2,6-bis(1H-indol-3-yl)-1,4-dihydropyridine-3,5-dicarbonitrile ethanol monosolvateSong-Lei ZhuJun-Nian ZhengIn the title compound, C29H18ClN5·C2H6O, the dihydropyridine ring adopts a strongly flattened envelope conformation, with a maximum deviation of 0.139 (2) Å from its best plane for the Csp3 atom. The dihedral angles between the dihydropyridine ring plane and the two indole rings in positions 2 and 6 are 34.28 (5) and 40.50 (6)°, respectively. In turn, the benzene ring and the dihydropyridine ring are oriented at a dihedral angle of 74.69 (6)°. An intramolecular C—H...Cl hydrogen bond occurs. In the crystal, molecules are linked by N—H...N, N—H...O and O—H...N hydrogen bonds into layers parallel to (001). There are short C—H...Cl contacts between molecules in neighboring layers.http://scripts.iucr.org/cgi-bin/paper?S1600536812013906
collection DOAJ
language English
format Article
sources DOAJ
author Song-Lei Zhu
Jun-Nian Zheng
spellingShingle Song-Lei Zhu
Jun-Nian Zheng
4-(4-Chlorophenyl)-2,6-bis(1H-indol-3-yl)-1,4-dihydropyridine-3,5-dicarbonitrile ethanol monosolvate
Acta Crystallographica Section E
author_facet Song-Lei Zhu
Jun-Nian Zheng
author_sort Song-Lei Zhu
title 4-(4-Chlorophenyl)-2,6-bis(1H-indol-3-yl)-1,4-dihydropyridine-3,5-dicarbonitrile ethanol monosolvate
title_short 4-(4-Chlorophenyl)-2,6-bis(1H-indol-3-yl)-1,4-dihydropyridine-3,5-dicarbonitrile ethanol monosolvate
title_full 4-(4-Chlorophenyl)-2,6-bis(1H-indol-3-yl)-1,4-dihydropyridine-3,5-dicarbonitrile ethanol monosolvate
title_fullStr 4-(4-Chlorophenyl)-2,6-bis(1H-indol-3-yl)-1,4-dihydropyridine-3,5-dicarbonitrile ethanol monosolvate
title_full_unstemmed 4-(4-Chlorophenyl)-2,6-bis(1H-indol-3-yl)-1,4-dihydropyridine-3,5-dicarbonitrile ethanol monosolvate
title_sort 4-(4-chlorophenyl)-2,6-bis(1h-indol-3-yl)-1,4-dihydropyridine-3,5-dicarbonitrile ethanol monosolvate
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2012-05-01
description In the title compound, C29H18ClN5·C2H6O, the dihydropyridine ring adopts a strongly flattened envelope conformation, with a maximum deviation of 0.139 (2) Å from its best plane for the Csp3 atom. The dihedral angles between the dihydropyridine ring plane and the two indole rings in positions 2 and 6 are 34.28 (5) and 40.50 (6)°, respectively. In turn, the benzene ring and the dihydropyridine ring are oriented at a dihedral angle of 74.69 (6)°. An intramolecular C—H...Cl hydrogen bond occurs. In the crystal, molecules are linked by N—H...N, N—H...O and O—H...N hydrogen bonds into layers parallel to (001). There are short C—H...Cl contacts between molecules in neighboring layers.
url http://scripts.iucr.org/cgi-bin/paper?S1600536812013906
work_keys_str_mv AT songleizhu 44chlorophenyl26bis1hindol3yl14dihydropyridine35dicarbonitrileethanolmonosolvate
AT junnianzheng 44chlorophenyl26bis1hindol3yl14dihydropyridine35dicarbonitrileethanolmonosolvate
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