Microstructural Stability of Extruded Mg-Mn-Ce Hollow Profiles with Weld Seams

• Main Authors: Felix Gensch, Sven Gall, Stefan Lechner, Christoph Fahrenson, Soeren Mueller
• Format: Article
• Language: English
• Published: MDPI AG 2021-03-01
• Series: Metals
• Subjects: extrusion; magnesium; weld seams; rare-earth; heat treatment; electron backscatter diffraction (EBSD)
• Online Access: https://www.mdpi.com/2075-4701/11/4/547

Despite aluminum profiles, magnesium profiles have not been well developed due to the low formability. Furthermore, extruded magnesium profiles show a strong dependence on the mechanical properties, according to the loading direction. This is caused by a strong basal texture, which is directly dependent on the process parameters during the extrusion and the subsequent aging. Thus, the present paper focuses on the analysis of the microstructure and its evolution of extruded magnesium hollow profiles, which were subjected to a series of heat treatments at 475 °C up to one hour. The hollow profiles were extruded through a porthole die, thus, containing longitudinal weld seams. These were formed by material that underwent heavy shearing along the tool surface based on the friction conditions in the porthole die. Three extrusion ratios (ER = 8:1, ER = 16:1, ER = 30:1) were applied, resulting in three different wall thicknesses of the profiles. The microstructure of the profiles was analyzed using light-optical microscopy (LOM) and scanning electron microscopy (SEM) coupled with electron backscatter diffraction (EBSD). The analysis revealed no change of the microstructure of the profiles extruded at the two higher extrusion ratios within the time frame of the heat treatment. In contrast, the microstructure and, thus, the micro-texture of the profile with the lowest extrusion ratio (ER = 8:1) has been affected to a great extent. While only small changes in microstructure in the weld-free area were observed, the initial microstructure in the weld seam was transformed from fine recrystallized grains into a significantly bimodal microstructure mainly due to an abnormal grain growth (AGG). These changes were accompanied by a promotion of the rare-earth (RE) texture component for the weld-free material and a change of the overall texture from RE to a typical non-RE double fiber texture for the weld seam due to the intense AGG within the short-time heat treatments. In addition, the influence of the extrusion ratio on particle size and distribution as well as the character of the microstructure governing the behavior during heat treatments was analyzed and discussed.